C₅₉H₉₀INO₉Si₂

Base Information

Chemical Name:C₅₉H₉₀INO₉Si₂
CAS No.:1378890-10-8
Molecular Formula:C₅₉H₉₀INO₉Si₂
Molecular Weight:1140.44
Hs Code.:

C<sub>59</sub>H<sub>90</sub>INO<sub>9</sub>Si<sub>2</sub>

Synonyms:C₅₉H₉₀INO₉Si₂

Suppliers and Price of C₅₉H₉₀INO₉Si₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₅₉H₉₀INO₉Si₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₅₉H₉₀INO₉Si₂

There total 13 articles about C₅₉H₉₀INO₉Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: C₅₉H₈₈INO₉Si₂

: 1378890-10-8
C₅₉H₉₀INO₉Si₂

Guidance literature:: With (triphenylphosphine)copper(I) hydride hexamer; In benzene; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1021/ol301103d

Reference yield:

: 1269618-49-6
C₂₇H₄₁O₆PSi

: 1378890-10-8
C₅₉H₉₀INO₉Si₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: barium hydroxide octahydrate / tetrahydrofuran; water / 0.5 h / 20 °C / Inert atmosphere

1.2: 6 h / 20 °C / Inert atmosphere

2.1: (triphenylphosphine)copper(I) hydride hexamer / benzene / 6 h / 20 °C / Inert atmosphere

With (triphenylphosphine)copper(I) hydride hexamer; barium hydroxide octahydrate; In tetrahydrofuran; water; benzene; 1.1: Horner-Wadsworth-Emmons olefination / 1.2: Horner-Wadsworth-Emmons olefination;
DOI:10.1021/ol301103d

Reference yield:

: C₄₃H₆₆O₇Si₂

: 1378890-10-8
C₅₉H₉₀INO₉Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

1.2: 12 h / 20 °C / Inert atmosphere

2.1: sodium hydrogencarbonate; Dess-Martin periodane; tert-butyl alcohol / dichloromethane / 0.75 h / Inert atmosphere

3.1: 2,6-di-tert-butyl-4-methylpyridine; 1,2-dibromo-1,1,2,2-tetrachloroethane; triphenylphosphine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

3.2: 3 h / 20 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran; N,N-dimethyl-formamide / 6.08 h / 0 - 20 °C / Inert atmosphere

5.1: barium hydroxide octahydrate / tetrahydrofuran; water / 0.5 h / 20 °C / Inert atmosphere

5.2: 6 h / 20 °C / Inert atmosphere

6.1: (triphenylphosphine)copper(I) hydride hexamer / benzene / 6 h / 20 °C / Inert atmosphere

With 2,6-di-tert-butyl-4-methylpyridine; (triphenylphosphine)copper(I) hydride hexamer; barium hydroxide octahydrate; 1,2-dibromo-1,1,2,2-tetrachloroethane; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; Dess-Martin periodane; acetic acid; triethylamine; triphenylphosphine; tert-butyl alcohol; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; benzene; 2.1: Dess-Martin oxidation / 5.1: Horner-Wadsworth-Emmons olefination / 5.2: Horner-Wadsworth-Emmons olefination;
DOI:10.1021/ol301103d