Technology Process of C22H26Cl2N3O11P
There total 5 articles about C22H26Cl2N3O11P which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridinium p-toluenesulfonate;
In
water; acetone;
for 5h;
Reflux;
DOI:10.1021/ja411733s
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 5-(ethylthio)-1H-tetrazole / acetonitrile / 1 h / 25 °C / Inert atmosphere
1.2: 0.33 h / Inert atmosphere
2.1: hydrazine / tetrahydrofuran; water / 0.08 h / 25 °C
3.1: acetic acid / dimethyl sulfoxide / 37 °C
4.1: pyridinium p-toluenesulfonate / water; acetone / 5 h / Reflux
With
pyridinium p-toluenesulfonate; acetic acid; 5-(ethylthio)-1H-tetrazole; hydrazine;
In
tetrahydrofuran; water; dimethyl sulfoxide; acetone; acetonitrile;
DOI:10.1021/ja411733s
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrazine / tetrahydrofuran; water / 0.08 h / 25 °C
2: acetic acid / dimethyl sulfoxide / 37 °C
3: pyridinium p-toluenesulfonate / water; acetone / 5 h / Reflux
With
pyridinium p-toluenesulfonate; acetic acid; hydrazine;
In
tetrahydrofuran; water; dimethyl sulfoxide; acetone;
DOI:10.1021/ja411733s