Technology Process of C28H38O7S
There total 7 articles about C28H38O7S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 5 steps
1: pyridinium dichromate / N,N-dimethyl-formamide
2: potassium hydroxide / methanol / 20 °C
3: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane
4: dmap / pyridine
5: palladium 10% on activated carbon; hydrogen / ethanol
With
dmap; pyridinium dichromate; palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide;
In
pyridine; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
3: Baeyer-Villiger oxidation;
DOI:10.1016/j.bmcl.2012.01.051
- Guidance literature:
-
Multi-step reaction with 6 steps
1: dmap; triethylamine / tetrahydrofuran / 0.75 h
2: pyridinium dichromate / N,N-dimethyl-formamide
3: potassium hydroxide / methanol / 20 °C
4: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane
5: dmap / pyridine
6: palladium 10% on activated carbon; hydrogen / ethanol
With
dmap; pyridinium dichromate; palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide;
In
tetrahydrofuran; pyridine; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
4: Baeyer-Villiger oxidation;
DOI:10.1016/j.bmcl.2012.01.051