Technology Process of C24H34FN7O6
There total 8 articles about C24H34FN7O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: tin(II) chloride dihdyrate / ethanol / 2 h / 80 - 90 °C
1.2: 80 - 90 °C
2.1: sodium carbonate / 17 h / 20 °C
3.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C
3.2: -78 - 20 °C
3.3: 6 h / 20 °C
4.1: hydrogen / palladium 10% on activated carbon / methanol; water / 7.5 h / 20 °C
5.1: sodium carbonate / methanol / 24 h / 20 °C
6.1: triethylamine / chloroform / Cooling with ice
7.1: sodium azide / N,N-dimethyl-formamide / 10 h / 60 °C
With
n-butyllithium; sodium azide; tin(II) chloride dihdyrate; hydrogen; sodium carbonate; triethylamine;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; ethanol; hexane; chloroform; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C
1.2: -78 - 20 °C
1.3: 6 h / 20 °C
2.1: hydrogen / palladium 10% on activated carbon / methanol; water / 7.5 h / 20 °C
3.1: sodium carbonate / methanol / 24 h / 20 °C
4.1: triethylamine / chloroform / Cooling with ice
5.1: sodium azide / N,N-dimethyl-formamide / 10 h / 60 °C
With
n-butyllithium; sodium azide; hydrogen; sodium carbonate; triethylamine;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; hexane; chloroform; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium carbonate / 17 h / 20 °C
2.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C
2.2: -78 - 20 °C
2.3: 6 h / 20 °C
3.1: hydrogen / palladium 10% on activated carbon / methanol; water / 7.5 h / 20 °C
4.1: sodium carbonate / methanol / 24 h / 20 °C
5.1: triethylamine / chloroform / Cooling with ice
6.1: sodium azide / N,N-dimethyl-formamide / 10 h / 60 °C
With
n-butyllithium; sodium azide; hydrogen; sodium carbonate; triethylamine;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; hexane; chloroform; water; N,N-dimethyl-formamide;