tert-butyl N-glycylanthranilate hydrochloride

Base Information

Chemical Name:tert-butyl N-glycylanthranilate hydrochloride
CAS No.:106880-83-5
Molecular Formula:C₁₃H₁₈N₂O₃*ClH
Molecular Weight:286.758
Hs Code.:

Synonyms:tert-butyl N-glycylanthranilate hydrochloride

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Chemical Property of tert-butyl N-glycylanthranilate hydrochloride

Chemical Property:

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Technology Process of tert-butyl N-glycylanthranilate hydrochloride

There total 4 articles about tert-butyl N-glycylanthranilate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 106880-81-3
benzyl <<<(tert-butoxycarbonyl)phenyl>carbamoyl>methyl>carbamate

: 106880-83-5
tert-butyl N-glycylanthranilate hydrochloride

Guidance literature:: With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol; for 0.666667h; Ambient temperature;
DOI:10.1021/ja00240a036

Reference yield:

: 19165-29-8
N-(trifluoroacetyl)anthranilic acid

: 106880-83-5
tert-butyl N-glycylanthranilate hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) N,N'-carbonylbisimidazole / 1.) 2 h, RT; 2.) tert-butyl alcohol, 36 h, RT, and ethanol, sodium borohydride, 0 deg C, ca. 25 min

2: 80 percent / N-ethyl-N'-((dimethylamino)propyl)carbodiimide hydrochloride / CH₂Cl₂ / 168 h / Ambient temperature

3: 92 percent / 1.) H₂; 2.) cc. HCl / 10 percent Pd-C / ethanol / 0.67 h / Ambient temperature

With hydrogenchloride; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1,1'-carbonyldiimidazole; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1021/ja00240a036

Reference yield:

: 64113-91-3
tert-butyl 2-aminobenzoate

: 106880-83-5
tert-butyl N-glycylanthranilate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / N-ethyl-N'-((dimethylamino)propyl)carbodiimide hydrochloride / CH₂Cl₂ / 168 h / Ambient temperature

2: 92 percent / 1.) H₂; 2.) cc. HCl / 10 percent Pd-C / ethanol / 0.67 h / Ambient temperature

With hydrogenchloride; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1021/ja00240a036