3-<1-(p-fluorophenylhydrazono)-D-erythro-2,3,4-trihydroxybutyl>-1-methyl-2-quinoxalinone

Base Information

Chemical Name:3-<1-(p-fluorophenylhydrazono)-D-erythro-2,3,4-trihydroxybutyl>-1-methyl-2-quinoxalinone
CAS No.:105291-54-1
Molecular Formula:C₁₉H₁₉FN₄O₄
Molecular Weight:386.383
Hs Code.:

Synonyms:3-<1-(p-fluorophenylhydrazono)-D-erythro-2,3,4-trihydroxybutyl>-1-methyl-2-quinoxalinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-<1-(p-fluorophenylhydrazono)-D-erythro-2,3,4-trihydroxybutyl>-1-methyl-2-quinoxalinone

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Technology Process of 3-<1-(p-fluorophenylhydrazono)-D-erythro-2,3,4-trihydroxybutyl>-1-methyl-2-quinoxalinone

There total 4 articles about 3-<1-(p-fluorophenylhydrazono)-D-erythro-2,3,4-trihydroxybutyl>-1-methyl-2-quinoxalinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 75-93-4
methyl bisulfate

: 105291-50-7
3-<1-(p-fluorophenylhydrazono)-D-erythro-2,3,4-trihydroxybutyl>-2-quinoxalinone

: 105291-54-1
3-<1-(p-fluorophenylhydrazono)-D-erythro-2,3,4-trihydroxybutyl>-1-methyl-2-quinoxalinone

Guidance literature:: With sodium hydroxide; In ethanol; for 10h; Ambient temperature;
DOI:10.1016/S0008-6215(00)90318-5

Reference yield:

: 371-14-2
4-fluorophenylhydrazine

: 105291-54-1
3-<1-(p-fluorophenylhydrazono)-D-erythro-2,3,4-trihydroxybutyl>-1-methyl-2-quinoxalinone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) p-benzoquinone / 1.) ethanol, r.t., 1.5 h; 2.) ethanol, water, reflux, 5-10 min

2: 78 percent / sodium hydroxide / aq. ethanol / 10 h / Ambient temperature

With sodium hydroxide; p-benzoquinone; In ethanol;
DOI:10.1016/S0008-6215(00)90318-5

Reference yield:

: 95-54-5
1,2-diamino-benzene

: 105291-54-1
3-<1-(p-fluorophenylhydrazono)-D-erythro-2,3,4-trihydroxybutyl>-1-methyl-2-quinoxalinone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) p-benzoquinone / 1.) ethanol, r.t., 1.5 h; 2.) ethanol, water, reflux, 5-10 min

2: 78 percent / sodium hydroxide / aq. ethanol / 10 h / Ambient temperature

With sodium hydroxide; p-benzoquinone; In ethanol;
DOI:10.1016/S0008-6215(00)90318-5