diethyl 2-((R)-4-amino-5-(benzyloxy)-5-oxopentanamido)-6-((tert-butoxycarbonyl)amino)heptanedioate

Base Information

Chemical Name:diethyl 2-((R)-4-amino-5-(benzyloxy)-5-oxopentanamido)-6-((tert-butoxycarbonyl)amino)heptanedioate
CAS No.:1269619-88-6
Molecular Formula:C₂₈H₄₃N₃O₉
Molecular Weight:565.664
Hs Code.:

Synonyms:diethyl 2-((R)-4-amino-5-(benzyloxy)-5-oxopentanamido)-6-((tert-butoxycarbonyl)amino)heptanedioate

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Chemical Property of diethyl 2-((R)-4-amino-5-(benzyloxy)-5-oxopentanamido)-6-((tert-butoxycarbonyl)amino)heptanedioate

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Technology Process of diethyl 2-((R)-4-amino-5-(benzyloxy)-5-oxopentanamido)-6-((tert-butoxycarbonyl)amino)heptanedioate

There total 13 articles about diethyl 2-((R)-4-amino-5-(benzyloxy)-5-oxopentanamido)-6-((tert-butoxycarbonyl)amino)heptanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1269619-54-6
(5R)-5-benzyl 10,14-diethyl-1-(9H-fluoren-9-yl)-18,18-dimethyl-3,8,16-trioxo-2,17-dioxa-4,9,15-triazanonadecane-5,10,14-tricarboxylate

: 1269619-88-6
diethyl 2-((R)-4-amino-5-(benzyloxy)-5-oxopentanamido)-6-((tert-butoxycarbonyl)amino)heptanedioate

Guidance literature:: With piperidine; In dichloromethane; for 0.25h;
DOI:10.1021/jm101535e

Reference yield:

: 1269619-50-2
diethyl 2-amino-6-((tert-butoxycarbonyl)amino)heptanedioate

: 1269619-88-6
diethyl 2-((R)-4-amino-5-(benzyloxy)-5-oxopentanamido)-6-((tert-butoxycarbonyl)amino)heptanedioate

Guidance literature:: Multi-step reaction with 2 steps

1: polystyrene bound carbodiimide; polystyrene bound DMAP / dichloromethane / 4 h / 20 °C

2: piperidine / dichloromethane / 0.25 h

With piperidine; In dichloromethane;
DOI:10.1021/jm101535e

Reference yield:

: 6305-09-5
C₁₁H₂₂N₂O₄*ClH

: 1269619-88-6
diethyl 2-((R)-4-amino-5-(benzyloxy)-5-oxopentanamido)-6-((tert-butoxycarbonyl)amino)heptanedioate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / methanol / 0.5 h / pH 7

2: polystyrene bound carbodiimide; polystyrene bound DMAP / dichloromethane / 4 h / 20 °C

3: piperidine / dichloromethane / 0.25 h

With piperidine; triethylamine; In methanol; dichloromethane;
DOI:10.1021/jm101535e