C₂₂H₃₄O₆

Base Information

Chemical Name:C₂₂H₃₄O₆
CAS No.:1410659-70-9
Molecular Formula:C₂₂H₃₄O₆
Molecular Weight:394.508
Hs Code.:

C<sub>22</sub>H<sub>34</sub>O<sub>6</sub>

Synonyms:C₂₂H₃₄O₆

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Chemical Property of C₂₂H₃₄O₆

Chemical Property:

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Technology Process of C₂₂H₃₄O₆

There total 8 articles about C₂₂H₃₄O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 547-63-7,133320-07-7,67505-84-4
Methyl isobutyrate

: 1410659-50-5
C₁₇H₂₄O₄

: 1410659-68-5
C₂₂H₃₄O₆

: 1410659-70-9
C₂₂H₃₄O₆

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃;
DOI:10.1016/j.tetlet.2012.07.043 DOI:10.1016/j.tetlet.2012.07.043

Reference yield:

: C₁₉H₂₈O₅

: 1410659-70-9
C₂₂H₃₄O₆

Guidance literature:: Multi-step reaction with 7 steps

1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran / Inert atmosphere

2: toluene-4-sulfonic acid / methanol / Inert atmosphere

3: triethylamine / dichloromethane / Inert atmosphere

4: toluene-4-sulfonic acid / dichloromethane / Inert atmosphere

5: potassium carbonate / methanol / Inert atmosphere

6: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / Inert atmosphere

7: lithium diisopropyl amide / tetrahydrofuran / -78 °C

With sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; toluene-4-sulfonic acid; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; lithium diisopropyl amide; In tetrahydrofuran; methanol; dichloromethane; 7: |Aldol Condensation;
DOI:10.1016/j.tetlet.2012.07.043 DOI:10.1016/j.tetlet.2012.07.043

Reference yield:

: 1410659-57-2
C₁₉H₂₈O₄

: 1410659-70-9
C₂₂H₃₄O₆

Guidance literature:: Multi-step reaction with 8 steps

1: L-(+)-diisopropyl tartrate; titanium(IV) isopropylate; tert.-butylhydroperoxide / dichloromethane / -20 °C / Inert atmosphere

2: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran / Inert atmosphere

3: toluene-4-sulfonic acid / methanol / Inert atmosphere

4: triethylamine / dichloromethane / Inert atmosphere

5: toluene-4-sulfonic acid / dichloromethane / Inert atmosphere

6: potassium carbonate / methanol / Inert atmosphere

7: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / Inert atmosphere

8: lithium diisopropyl amide / tetrahydrofuran / -78 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; toluene-4-sulfonic acid; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; lithium diisopropyl amide; In tetrahydrofuran; methanol; dichloromethane; 1: |Sharpless Asymmetric Epoxidation / 8: |Aldol Condensation;
DOI:10.1016/j.tetlet.2012.07.043 DOI:10.1016/j.tetlet.2012.07.043