2-O-acetyl-6-O-benzyl-4-O-para-bromobenzyl-3-O-tert-butyldimethylsilyl-7-O-tert-butyldiphenylsilyl-L-glycero-α/β-D-manno-heptopyranosyl N-phenyl-trifluoroacetimidate

Base Information

Chemical Name:2-O-acetyl-6-O-benzyl-4-O-para-bromobenzyl-3-O-tert-butyldimethylsilyl-7-O-tert-butyldiphenylsilyl-L-glycero-α/β-D-manno-heptopyranosyl N-phenyl-trifluoroacetimidate
CAS No.:1237498-89-3
Molecular Formula:C₅₃H₆₃BrF₃NO₈Si₂
Molecular Weight:1035.16
Hs Code.:

2-O-acetyl-6-O-benzyl-4-O-para-bromobenzyl-3-O-tert-butyldimethylsilyl-7-O-tert-butyldiphenylsilyl-L-glycero-α/β-D-manno-heptopyranosyl N-phenyl-trifluoroacetimidate

Synonyms:2-O-acetyl-6-O-benzyl-4-O-para-bromobenzyl-3-O-tert-butyldimethylsilyl-7-O-tert-butyldiphenylsilyl-L-glycero-α/β-D-manno-heptopyranosyl N-phenyl-trifluoroacetimidate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-O-acetyl-6-O-benzyl-4-O-para-bromobenzyl-3-O-tert-butyldimethylsilyl-7-O-tert-butyldiphenylsilyl-L-glycero-α/β-D-manno-heptopyranosyl N-phenyl-trifluoroacetimidate

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Technology Process of 2-O-acetyl-6-O-benzyl-4-O-para-bromobenzyl-3-O-tert-butyldimethylsilyl-7-O-tert-butyldiphenylsilyl-L-glycero-α/β-D-manno-heptopyranosyl N-phenyl-trifluoroacetimidate

There total 1 articles about 2-O-acetyl-6-O-benzyl-4-O-para-bromobenzyl-3-O-tert-butyldimethylsilyl-7-O-tert-butyldiphenylsilyl-L-glycero-α/β-D-manno-heptopyranosyl N-phenyl-trifluoroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 2-O-acetyl-6-O-benzyl-4-O-para-bromobenzyl-3-O-tert-butyldimethylsilyl-7-O-tert-butyldiphenylsilyl-L-glycero-α/β-D-manno-heptopyranose

: 61881-19-4
2,2,2-trifluoro-N-phenyl-acetimidoyl chloride

: 1237498-89-3
2-O-acetyl-6-O-benzyl-4-O-para-bromobenzyl-3-O-tert-butyldimethylsilyl-7-O-tert-butyldiphenylsilyl-L-glycero-α/β-D-manno-heptopyranosyl N-phenyl-trifluoroacetimidate

Guidance literature:: With caesium carbonate; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c000784f

Reference yield:

: 1237498-92-8
N-benzyl-N-benzyloxycarbonyl-5-aminopentyl 2,7-O-di-acetyl-6-O-benzyl-4-O-para-bromobenzyl-L-glycero-α-D-manno-heptopyranoside

: 1237498-89-3
2-O-acetyl-6-O-benzyl-4-O-para-bromobenzyl-3-O-tert-butyldimethylsilyl-7-O-tert-butyldiphenylsilyl-L-glycero-α/β-D-manno-heptopyranosyl N-phenyl-trifluoroacetimidate

: C₉₀H₁₀₉Br₂NO₁₈Si₂

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -20 - 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1039/c000784f