C₃₁H₅₀O₄Si₂

Base Information

Chemical Name:C₃₁H₅₀O₄Si₂
CAS No.:948297-41-4
Molecular Formula:C₃₁H₅₀O₄Si₂
Molecular Weight:542.907
Hs Code.:

C<sub>31</sub>H<sub>50</sub>O<sub>4</sub>Si<sub>2</sub>

Synonyms:C₃₁H₅₀O₄Si₂

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Chemical Property of C₃₁H₅₀O₄Si₂

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Technology Process of C₃₁H₅₀O₄Si₂

There total 11 articles about C₃₁H₅₀O₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 105966-43-6
3-tert-butyldiphenylsilyloxy-2-methylpropene

: 948297-41-4
C₃₁H₅₀O₄Si₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: 89 percent / 2,2-di(S-4-tBu-4,5-dihydrooxazol-2-yl)propane Cu(II) complex / CH₂Cl₂ / 12 h

2.1: 98 percent / Me₃Al / tetrahydrofuran

3.1: 95 percent / NaH / dimethylformamide

4.1: 90 percent / tBuLi / diethyl ether / -78 °C

5.1: L-Selectride / tetrahydrofuran / -78 °C

6.1: O₃; pyridine / CH₂Cl₂; methanol / -78 °C

6.2: Me₂S / CH₂Cl₂; methanol / -78 - 20 °C

7.1: pyridinium p-toluenesulfonate

8.1: Et₃SiH; BF₃*OEt₂ / CH₂Cl₂ / -78 °C

9.1: 94 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / CH₂Cl₂ / 0 °C / pH 7

10.1: 97 percent / imidazole / dimethylformamide

11.1: 96 percent / lithium di-tert-butyl biphenylide / tetrahydrofuran / -78 °C

With pyridine; 1H-imidazole; triethylsilane; boron trifluoride diethyl etherate; trimethylaluminum; tert.-butyl lithium; pyridinium p-toluenesulfonate; L-Selectride; sodium hydride; lithium 4,4′-di-tert-butylbiphenylide; ozone; 2,3-dicyano-5,6-dichloro-p-benzoquinone; 2,2-di(S-4-tBu-4,5-dihydrooxazol-2-yl)propane Cu(II) complex; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.200701515

Reference yield:

: 948297-37-8
C₂₄H₃₃NO₄Si

: 948297-41-4
C₃₁H₅₀O₄Si₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: 95 percent / NaH / dimethylformamide

2.1: 90 percent / tBuLi / diethyl ether / -78 °C

3.1: L-Selectride / tetrahydrofuran / -78 °C

4.1: O₃; pyridine / CH₂Cl₂; methanol / -78 °C

4.2: Me₂S / CH₂Cl₂; methanol / -78 - 20 °C

5.1: pyridinium p-toluenesulfonate

6.1: Et₃SiH; BF₃*OEt₂ / CH₂Cl₂ / -78 °C

7.1: 94 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / CH₂Cl₂ / 0 °C / pH 7

8.1: 97 percent / imidazole / dimethylformamide

9.1: 96 percent / lithium di-tert-butyl biphenylide / tetrahydrofuran / -78 °C

With pyridine; 1H-imidazole; triethylsilane; boron trifluoride diethyl etherate; tert.-butyl lithium; pyridinium p-toluenesulfonate; L-Selectride; sodium hydride; lithium 4,4′-di-tert-butylbiphenylide; ozone; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.200701515

Reference yield:

: 948297-38-9
C₄₁H₅₀O₅Si

: 948297-41-4
C₃₁H₅₀O₄Si₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: L-Selectride / tetrahydrofuran / -78 °C

2.1: O₃; pyridine / CH₂Cl₂; methanol / -78 °C

2.2: Me₂S / CH₂Cl₂; methanol / -78 - 20 °C

3.1: pyridinium p-toluenesulfonate

4.1: Et₃SiH; BF₃*OEt₂ / CH₂Cl₂ / -78 °C

5.1: 94 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / CH₂Cl₂ / 0 °C / pH 7

6.1: 97 percent / imidazole / dimethylformamide

7.1: 96 percent / lithium di-tert-butyl biphenylide / tetrahydrofuran / -78 °C

With pyridine; 1H-imidazole; triethylsilane; boron trifluoride diethyl etherate; pyridinium p-toluenesulfonate; L-Selectride; lithium 4,4′-di-tert-butylbiphenylide; ozone; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.200701515