methyl 2β-formyl-3β<(benzyloxycarbonyl)amino>-4-cyclohexene-α-carboxylate

Base Information

Chemical Name:methyl 2β-formyl-3β<(benzyloxycarbonyl)amino>-4-cyclohexene-α-carboxylate
CAS No.:77823-89-3
Molecular Formula:C₁₇H₁₉NO₅
Molecular Weight:317.342
Hs Code.:

Synonyms:methyl 2β-formyl-3β<(benzyloxycarbonyl)amino>-4-cyclohexene-α-carboxylate

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Chemical Property of methyl 2β-formyl-3β<(benzyloxycarbonyl)amino>-4-cyclohexene-α-carboxylate

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Technology Process of methyl 2β-formyl-3β<(benzyloxycarbonyl)amino>-4-cyclohexene-α-carboxylate

There total 1 articles about methyl 2β-formyl-3β<(benzyloxycarbonyl)amino>-4-cyclohexene-α-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 5837-72-9
methyl (E)-4-oxo-2-butenoate

: 65899-49-2
1(E)-<(benzyloxycarbonyl)amino>-1,3-butadiene

: 77823-89-3
methyl 2β-formyl-3β<(benzyloxycarbonyl)amino>-4-cyclohexene-α-carboxylate

Guidance literature:: In toluene; for 3h; Heating;
DOI:10.1021/jm00139a005

Reference yield: 92.0%

: 77823-89-3
methyl 2β-formyl-3β<(benzyloxycarbonyl)amino>-4-cyclohexene-α-carboxylate

: 2136-75-6
(triphenylphosphoranylidene)acetaldehyde

: 77823-90-6,98819-46-6,98819-47-7
methyl 2β-<3-oxo-2(E)-propenyl>-3β<(benzyloxycarbonyl)amino>-4-cyclohexene-α-carboxylate

Guidance literature:: In toluene; for 2h; Heating;
DOI:10.1021/jm00139a005

Reference yield:

: 77823-89-3
methyl 2β-formyl-3β<(benzyloxycarbonyl)amino>-4-cyclohexene-α-carboxylate

: 2136-75-6
(triphenylphosphoranylidene)acetaldehyde

: 99-33-2
3,5-dinitrobenoyl chloride

: 98761-73-0
(4aS,5S,8aS)-1-(3,5-Dinitro-benzoyl)-decahydro-quinoline-5-carboxylic acid methyl ester

: 98761-74-1
(4aS,5R,8aS)-1-(3,5-Dinitro-benzoyl)-decahydro-quinoline-5-carboxylic acid methyl ester

Guidance literature:: With hydrogen; dimethyl sulfoxide; palladium on activated charcoal; Yield given; 1.) 130 deg C, 10 h;
DOI:10.1021/jm00151a001