[7-methoxy-6-(3-methylbut-2-enyl)-2,2-diphenylbenzo[1,3]dioxol-5-yl]methanol

Base Information

• Chemical Name: [7-methoxy-6-(3-methylbut-2-enyl)-2,2-diphenylbenzo[1,3]dioxol-5-yl]methanol
• CAS No.: 1192659-09-8
• Molecular Formula: C₂₆H₂₆O₄
• Molecular Weight: 402.49

Synonyms:[7-methoxy-6-(3-methylbut-2-enyl)-2,2-diphenylbenzo[1,3]dioxol-5-yl]methanol

Chemical Property of [7-methoxy-6-(3-methylbut-2-enyl)-2,2-diphenylbenzo[1,3]dioxol-5-yl]methanol

Chemical Property:

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Technology Process of [7-methoxy-6-(3-methylbut-2-enyl)-2,2-diphenylbenzo[1,3]dioxol-5-yl]methanol

There total 1 articles about [7-methoxy-6-(3-methylbut-2-enyl)-2,2-diphenylbenzo[1,3]dioxol-5-yl]methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

7-methoxy-6-(3-methylbut-2-enyl)-2,2-diphenylbenzo[1,3]dioxole-5-carboxylic acid methyl ester (1192659-08-7) → [7-methoxy-6-(3-methylbut-2-enyl)-2,2-diphenylbenzo[1,3]dioxol-5-yl]methanol (1192659-09-8)

Guidance literature:

7-methoxy-6-(3-methylbut-2-enyl)-2,2-diphenylbenzo[1,3]dioxole-5-carboxylic acid methyl ester; With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃;

With water; ethyl acetate; In tetrahydrofuran;

DOI:10.1016/j.tet.2009.08.015

Reference yield:

[7-methoxy-6-(3-methylbut-2-enyl)-2,2-diphenylbenzo[1,3]dioxol-5-yl]methanol (1192659-09-8) → C26H25ClO3

Guidance literature:

With thionyl chloride; In benzene; at 70 ℃;

DOI:10.1016/j.tet.2009.08.015

upstream raw materials:

7-methoxy-6-(3-methylbut-2-enyl)-2,2-diphenylbenzo[1,3]dioxole-5-carboxylic acid methyl ester

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