C₁₃H₁₅Cl₂NO₂

Base Information

• Chemical Name: C₁₃H₁₅Cl₂NO₂
• CAS No.: 1403595-49-2
• Molecular Formula: C₁₃H₁₅Cl₂NO₂
• Molecular Weight: 288.174
• Mol file: 1403595-49-2.mol

Synonyms:C₁₃H₁₅Cl₂NO₂

Chemical Property of C₁₃H₁₅Cl₂NO₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₁₃H₁₅Cl₂NO₂

There total 4 articles about C₁₃H₁₅Cl₂NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

methyl 2,5-dichloro-3-(cyclopentyl(methyl)amino)benzoate (1403595-48-1) → C13H15Cl2NO2 (1403595-49-2)

Guidance literature:

methyl 2,5-dichloro-3-(cyclopentyl(methyl)amino)benzoate; With water; sodium hydroxide; In methanol; at 60 ℃; for 1h;

With hydrogenchloride; citric acid; In methanol; water; pH=4 - 6;

Reference yield:

methyl 2,5-dichloro-3-nitrobenzoate (34408-25-8) → C13H15Cl2NO2 (1403595-49-2)

Guidance literature:

Multi-step reaction with 4 steps

1.1: water; ammonium chloride; iron / ethanol / 3 h / 80 °C

2.1: acetic acid / methanol / 3 h / 20 °C

3.1: caesium carbonate / acetonitrile / 18 h / 80 °C

4.1: sodium hydroxide; water / methanol / 1 h / 60 °C

4.2: pH 4 - 6

With water; iron; ammonium chloride; caesium carbonate; acetic acid; sodium hydroxide; In methanol; ethanol; acetonitrile;

Reference yield:

2,5-dichloro-3-nitrobenzoic acid (88-86-8) → C13H15Cl2NO2 (1403595-49-2)

Guidance literature:

Multi-step reaction with 5 steps

1.1: sodium carbonate / N,N-dimethyl-formamide / 18 h / 60 °C

2.1: water; ammonium chloride; iron / ethanol / 3 h / 80 °C

3.1: acetic acid / methanol / 3 h / 20 °C

4.1: caesium carbonate / acetonitrile / 18 h / 80 °C

5.1: sodium hydroxide; water / methanol / 1 h / 60 °C

5.2: pH 4 - 6

With water; iron; sodium carbonate; ammonium chloride; caesium carbonate; acetic acid; sodium hydroxide; In methanol; ethanol; N,N-dimethyl-formamide; acetonitrile;

upstream raw materials:

methyl 2,5-dichloro-3-aminobenzoate

methyl 2,5-dichloro-3-nitrobenzoate

2,5-dichloro-3-nitrobenzoic acid

methyl 2,5-dichloro-3-(cyclopentyl(methyl)amino)benzoate