4-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)-(N-tert-butoxycarbonyl)phenylhydrazine

Base Information

Chemical Name:4-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)-(N-tert-butoxycarbonyl)phenylhydrazine
CAS No.:145839-36-7
Molecular Formula:C₄₂H₄₆N₂O₆
Molecular Weight:674.837
Hs Code.:

Synonyms:4-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)-(N-tert-butoxycarbonyl)phenylhydrazine

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Chemical Property of 4-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)-(N-tert-butoxycarbonyl)phenylhydrazine

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Technology Process of 4-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)-(N-tert-butoxycarbonyl)phenylhydrazine

There total 7 articles about 4-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)-(N-tert-butoxycarbonyl)phenylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 145839-40-3
2-(2-(2-(4-tritylphenoxy)ethoxy)ethoxy)ethyl 4-methylbenzenesulfonate

: 145839-39-0
4-hydroxy-(N-tert-butoxycarbonyl)phenylhydrazine

: 145839-36-7
4-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)-(N-tert-butoxycarbonyl)phenylhydrazine

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 60h;
DOI:10.1002/chem.19970030719

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 145839-36-7
4-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)-(N-tert-butoxycarbonyl)phenylhydrazine

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / Et₃N / methanol / 1 h / Heating

2: 91 percent / H₂ / 10percent Pd/C / ethanol / 4 h / Ambient temperature

3: 46 percent / K₂CO₃ / dimethylformamide / 60 h / 60 °C

With hydrogen; potassium carbonate; triethylamine; palladium on activated charcoal; In methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1002/chem.19970030719

Reference yield:

: 51145-58-5
[4-(benzyloxy)phenyl]hydrazine

: 145839-36-7
4-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)-(N-tert-butoxycarbonyl)phenylhydrazine

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / Et₃N / methanol / 1 h / Heating

2: 91 percent / H₂ / 10percent Pd/C / ethanol / 4 h / Ambient temperature

3: 46 percent / K₂CO₃ / dimethylformamide / 60 h / 60 °C

With hydrogen; potassium carbonate; triethylamine; palladium on activated charcoal; In methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1002/chem.19970030719