methyl 7,7-diphenyl-4-thiophen-3-yl-7λ⁵-phosphinino[2,3-b]furan-6-carboxylate

Base Information

Chemical Name:methyl 7,7-diphenyl-4-thiophen-3-yl-7λ⁵-phosphinino[2,3-b]furan-6-carboxylate
CAS No.:1448326-04-2
Molecular Formula:C₂₅H₁₉O₃PS
Molecular Weight:430.464
Hs Code.:

methyl 7,7-diphenyl-4-thiophen-3-yl-7λ<sup>5</sup>-phosphinino[2,3-b]furan-6-carboxylate

Synonyms:methyl 7,7-diphenyl-4-thiophen-3-yl-7λ⁵-phosphinino[2,3-b]furan-6-carboxylate

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Chemical Property of methyl 7,7-diphenyl-4-thiophen-3-yl-7λ⁵-phosphinino[2,3-b]furan-6-carboxylate

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Technology Process of methyl 7,7-diphenyl-4-thiophen-3-yl-7λ⁵-phosphinino[2,3-b]furan-6-carboxylate

There total 4 articles about methyl 7,7-diphenyl-4-thiophen-3-yl-7λ⁵-phosphinino[2,3-b]furan-6-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 67237-53-0
3-ethynylthiophene

: 1448325-79-8
[furan-2-yl(diphenyl)phosphonio](methoxycarbonyl)

: 1448326-04-2
methyl 7,7-diphenyl-4-thiophen-3-yl-7λ⁵-phosphinino[2,3-b]furan-6-carboxylate

Guidance literature:: In dichloromethane;
DOI:10.1016/j.tet.2013.06.066

Reference yield:

: 40927-82-0
diphenyl(2-furyl)phosphane

: 1448326-04-2
methyl 7,7-diphenyl-4-thiophen-3-yl-7λ⁵-phosphinino[2,3-b]furan-6-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: acetonitrile / 2 h / Reflux

2: sodium methylate / methanol / 2 h / 0 - 5 °C

3: methanol / 1 h / 0 - 5 °C

4: dichloromethane

With sodium methylate; In methanol; dichloromethane; acetonitrile;
DOI:10.1016/j.tet.2013.06.066

Reference yield:

: 1448325-73-2
furan-2-yl(2-methoxy-2-oxoethyl)diphenylphosphonium bromide

: 1448326-04-2
methyl 7,7-diphenyl-4-thiophen-3-yl-7λ⁵-phosphinino[2,3-b]furan-6-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium methylate / methanol / 2 h / 0 - 5 °C

2: methanol / 1 h / 0 - 5 °C

3: dichloromethane

With sodium methylate; In methanol; dichloromethane;
DOI:10.1016/j.tet.2013.06.066