N₁-[4-(4-bromophenylsulfonyl)benzoyl]-N₄-(3,4,5-trimethoxyphenyl)-thiosemicarbazide

Base Information

• Chemical Name: N₁-[4-(4-bromophenylsulfonyl)benzoyl]-N₄-(3,4,5-trimethoxyphenyl)-thiosemicarbazide
• CAS No.: 1361970-46-8
• Molecular Formula: C₂₃H₂₂BrN₃O₆S₂
• Molecular Weight: 580.48

Synonyms:N₁-[4-(4-bromophenylsulfonyl)benzoyl]-N₄-(3,4,5-trimethoxyphenyl)-thiosemicarbazide

Chemical Property of N₁-[4-(4-bromophenylsulfonyl)benzoyl]-N₄-(3,4,5-trimethoxyphenyl)-thiosemicarbazide

Chemical Property:

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Technology Process of N₁-[4-(4-bromophenylsulfonyl)benzoyl]-N₄-(3,4,5-trimethoxyphenyl)-thiosemicarbazide

There total 5 articles about N₁-[4-(4-bromophenylsulfonyl)benzoyl]-N₄-(3,4,5-trimethoxyphenyl)-thiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

(3,4,5-trimethoxyphenyl)isothiocyanate (35967-24-9) + p-(4-Bromophenylsulphonyl) benzoic acid hydrazide (20721-09-9) → N1-[4-(4-bromophenylsulfonyl)benzoyl]-N4-(3,4,5-trimethoxyphenyl)-thiosemicarbazide (1361970-46-8)

Guidance literature:

In ethanol; Reflux;

DOI:10.1016/j.ejmech.2012.01.031

Reference yield:

4-(4-bromo-benzenesulfonyl)-benzoic acid (96462-91-8) → N1-[4-(4-bromophenylsulfonyl)benzoyl]-N4-(3,4,5-trimethoxyphenyl)-thiosemicarbazide (1361970-46-8)

Guidance literature:

Multi-step reaction with 3 steps

1: sulfuric acid

2: hydrazine hydrate

3: ethanol / Reflux

With sulfuric acid; hydrazine hydrate; In ethanol;

DOI:10.1016/j.ejmech.2012.01.031

Reference yield:

bromobenzene (108-86-1,52753-63-6) → N1-[4-(4-bromophenylsulfonyl)benzoyl]-N4-(3,4,5-trimethoxyphenyl)-thiosemicarbazide (1361970-46-8)

Guidance literature:

Multi-step reaction with 5 steps

1: aluminum (III) chloride

2: chromium(VI) oxide; acetic acid

3: sulfuric acid

4: hydrazine hydrate

5: ethanol / Reflux

With chromium(VI) oxide; aluminum (III) chloride; sulfuric acid; hydrazine hydrate; acetic acid; In ethanol;

DOI:10.1016/j.ejmech.2012.01.031

upstream raw materials:

bromobenzene

1-bromo-4-tosylbenzene

(3,4,5-trimethoxyphenyl)isothiocyanate

p-(4-Bromophenylsulphonyl) benzoic acid hydrazide

Downstream raw materials:

5-(4-(4-bromophenylsulfonyl)phenyl)-4-(3,4,5-trimethoxyphenyl)-2H-1,2,4-triazol-3(4H)-thione

5-(4-(4-bromophenylsulfonyl)phenyl)-N-(3,4,5-trimethoxyphenyl)-1,3,4-thiadiazol-2-amine

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