({2-tert-Butoxycarbonylamino-3-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-propionylamino}-{(E)-2-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-vinylcarbamoyl}-methyl)-phosphonic acid dimethyl ester

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Chemical Name:({2-tert-Butoxycarbonylamino-3-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-propionylamino}-{(E)-2-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-vinylcarbamoyl}-methyl)-phosphonic acid dimethyl ester
CAS No.:121057-03-2
Molecular Formula:C₆₂H₁₁₈N₃O₁₃PSi₆
Molecular Weight:1313.12
Hs Code.:

({2-tert-Butoxycarbonylamino-3-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-propionylamino}-{(E)-2-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-vinylcarbamoyl}-methyl)-phosphonic acid dimethyl ester

Synonyms:({2-tert-Butoxycarbonylamino-3-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-propionylamino}-{(E)-2-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-vinylcarbamoyl}-methyl)-phosphonic acid dimethyl ester

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Chemical Property of ({2-tert-Butoxycarbonylamino-3-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-propionylamino}-{(E)-2-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-vinylcarbamoyl}-methyl)-phosphonic acid dimethyl ester

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Technology Process of ({2-tert-Butoxycarbonylamino-3-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-propionylamino}-{(E)-2-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-vinylcarbamoyl}-methyl)-phosphonic acid dimethyl ester

There total 19 articles about ({2-tert-Butoxycarbonylamino-3-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-propionylamino}-{(E)-2-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-vinylcarbamoyl}-methyl)-phosphonic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 121057-04-3
({2-tert-Butoxycarbonylamino-3-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-propionylamino}-{2-(4-nitro-phenylselanyl)-2-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-ethylcarbamoyl}-methyl)-phosphonic acid dimethyl ester

: 121057-03-2
({2-tert-Butoxycarbonylamino-3-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-propionylamino}-{(E)-2-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-vinylcarbamoyl}-methyl)-phosphonic acid dimethyl ester

Guidance literature:: With sodium periodate; In 1,4-dioxane; water; for 4.5h; Ambient temperature;
DOI:10.1021/ja00198a040

Reference yield:

: 99-24-1
methyl galloate

: 121057-03-2
({2-tert-Butoxycarbonylamino-3-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-propionylamino}-{(E)-2-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-vinylcarbamoyl}-methyl)-phosphonic acid dimethyl ester

Guidance literature:: Multi-step reaction with 10 steps

1: 93 percent / imidazole / dimethylformamide / 20 h

2: 79 percent / LiAlH₄ / tetrahydrofuran / 3 h / Heating

3: 75 percent / pyridinium chlorochromate / CH₂Cl₂ / 4 h / Ambient temperature

4: ZnI₂ / 4 h / Ambient temperature

5: LiAlH₄ / tetrahydrofuran / 3 h / Ambient temperature

6: 67 percent / CH₂Cl₂ / 0.5 h

7: 75 percent / tri-n-butylphosphine / tetrahydrofuran / 3 h / Ambient temperature

8: trifluoroacetic acid / CH₂Cl₂ / 1 h / Ambient temperature

9: 67 percent / Na₂SO₄, dicyclohexylcarbodiimide / ethyl acetate / 5 h / Ambient temperature

10: 61 percent / NaIO₄ / H₂O; dioxane / 4.5 h / Ambient temperature

With 1H-imidazole; sodium periodate; lithium aluminium tetrahydride; tributylphosphine; sodium sulfate; dicyclohexyl-carbodiimide; pyridinium chlorochromate; trifluoroacetic acid; zinc(II) iodide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/ja00198a040

Reference yield:

: 121056-97-1
methyl 3,4,5-tris<(tert-butyldimethylsilyl)oxy>benzoate

: 121057-03-2
({2-tert-Butoxycarbonylamino-3-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-propionylamino}-{(E)-2-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-vinylcarbamoyl}-methyl)-phosphonic acid dimethyl ester

Guidance literature:: Multi-step reaction with 9 steps

1: 79 percent / LiAlH₄ / tetrahydrofuran / 3 h / Heating

2: 75 percent / pyridinium chlorochromate / CH₂Cl₂ / 4 h / Ambient temperature

3: ZnI₂ / 4 h / Ambient temperature

4: LiAlH₄ / tetrahydrofuran / 3 h / Ambient temperature

5: 67 percent / CH₂Cl₂ / 0.5 h

6: 75 percent / tri-n-butylphosphine / tetrahydrofuran / 3 h / Ambient temperature

7: trifluoroacetic acid / CH₂Cl₂ / 1 h / Ambient temperature

8: 67 percent / Na₂SO₄, dicyclohexylcarbodiimide / ethyl acetate / 5 h / Ambient temperature

9: 61 percent / NaIO₄ / H₂O; dioxane / 4.5 h / Ambient temperature

With sodium periodate; lithium aluminium tetrahydride; tributylphosphine; sodium sulfate; dicyclohexyl-carbodiimide; pyridinium chlorochromate; trifluoroacetic acid; zinc(II) iodide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; ethyl acetate;
DOI:10.1021/ja00198a040