1,1-bis[3-(4'-methoxy-3'-methoxycarbonylbenzamido)-4-methoxy-5-methoxycarbonylphenyl]methane

Base Information

Chemical Name:1,1-bis[3-(4'-methoxy-3'-methoxycarbonylbenzamido)-4-methoxy-5-methoxycarbonylphenyl]methane
CAS No.:244262-30-4
Molecular Formula:C₃₉H₃₈N₂O₁₄
Molecular Weight:758.736
Hs Code.:

Synonyms:1,1-bis[3-(4'-methoxy-3'-methoxycarbonylbenzamido)-4-methoxy-5-methoxycarbonylphenyl]methane

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Chemical Property of 1,1-bis[3-(4'-methoxy-3'-methoxycarbonylbenzamido)-4-methoxy-5-methoxycarbonylphenyl]methane

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Technology Process of 1,1-bis[3-(4'-methoxy-3'-methoxycarbonylbenzamido)-4-methoxy-5-methoxycarbonylphenyl]methane

There total 3 articles about 1,1-bis[3-(4'-methoxy-3'-methoxycarbonylbenzamido)-4-methoxy-5-methoxycarbonylphenyl]methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 74121-10-1
4-methoxy-4-methoxycarbonylbenzoyl chloride

: 244262-25-7
1,1-bis(3-amino-4-methoxy-5-methoxycarbonylphenyl)methane

: 244262-30-4
1,1-bis[3-(4'-methoxy-3'-methoxycarbonylbenzamido)-4-methoxy-5-methoxycarbonylphenyl]methane

Guidance literature:: With pyridine; at 60 ℃;
DOI:10.1021/jo990177f

Reference yield:

: 207743-19-9
methyl 2-methoxy-5-{[4-methoxy-3-(methoxycarbonyl)phenyl]methyl}benzoate

: 244262-30-4
1,1-bis[3-(4'-methoxy-3'-methoxycarbonylbenzamido)-4-methoxy-5-methoxycarbonylphenyl]methane

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / HNO₃ / acetic anhydride / 0 - 20 °C

2: 78 percent / H₂ / PtO₂ / ethyl acetate / 4 h / 60 °C

3: 93 percent / pyridine / 60 °C

With pyridine; hydrogen; nitric acid; platinum(IV) oxide; In acetic anhydride; ethyl acetate; 1: Nitration / 2: Catalytic hydrogenation / 3: Acylation;
DOI:10.1021/jo990177f

Reference yield:

: 244262-21-3
1,1-bis(4-methoxy-3-methoxycarbonyl-5-nitrophenyl)methane

: 244262-30-4
1,1-bis[3-(4'-methoxy-3'-methoxycarbonylbenzamido)-4-methoxy-5-methoxycarbonylphenyl]methane

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / H₂ / PtO₂ / ethyl acetate / 4 h / 60 °C

2: 93 percent / pyridine / 60 °C

With pyridine; hydrogen; platinum(IV) oxide; In ethyl acetate; 1: Catalytic hydrogenation / 2: Acylation;
DOI:10.1021/jo990177f