Technology Process of C30H42O4
There total 6 articles about C30H42O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
methanol;
at 20 ℃;
for 7h;
Inert atmosphere;
DOI:10.1039/c1ob05251a
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: oxygen; palladium dichloride / N,N-dimethyl acetamide / 1 h / 20 °C / 9000.9 Torr
1.2: 12 h / 90 °C / 3000.3 Torr
2.1: lithium iodide / diethyl ether / 0.17 h / -40 °C / Inert atmosphere
2.2: 0.75 h / -100 °C / Inert atmosphere
2.3: -100 - 20 °C
3.1: sulfuric acid / 1,4-dioxane; water / 6 h / 20 °C / Reflux
4.1: potassium carbonate / methanol / 7 h / 20 °C / Inert atmosphere
With
sulfuric acid; oxygen; potassium carbonate; palladium dichloride; lithium iodide;
In
1,4-dioxane; methanol; diethyl ether; N,N-dimethyl acetamide; water;
DOI:10.1039/c1ob05251a
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium iodide / diethyl ether / 0.17 h / -40 °C / Inert atmosphere
1.2: 0.75 h / -100 °C / Inert atmosphere
1.3: -100 - 20 °C
2.1: sulfuric acid / 1,4-dioxane; water / 6 h / 20 °C / Reflux
3.1: potassium carbonate / methanol / 7 h / 20 °C / Inert atmosphere
With
sulfuric acid; potassium carbonate; lithium iodide;
In
1,4-dioxane; methanol; diethyl ether; water;
DOI:10.1039/c1ob05251a