bis(pentafluorophenyl)boron 1-[4-(dimethylamino)phenyl]-3-phenylpropane-1,3-dione

Base Information

Chemical Name:bis(pentafluorophenyl)boron 1-[4-(dimethylamino)phenyl]-3-phenylpropane-1,3-dione
CAS No.:1446682-13-8
Molecular Formula:C₂₉H₁₆BF₁₀NO₂
Molecular Weight:611.247
Hs Code.:

Synonyms:bis(pentafluorophenyl)boron 1-[4-(dimethylamino)phenyl]-3-phenylpropane-1,3-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(pentafluorophenyl)boron 1-[4-(dimethylamino)phenyl]-3-phenylpropane-1,3-dione

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Technology Process of bis(pentafluorophenyl)boron 1-[4-(dimethylamino)phenyl]-3-phenylpropane-1,3-dione

There total 4 articles about bis(pentafluorophenyl)boron 1-[4-(dimethylamino)phenyl]-3-phenylpropane-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 197009-46-4
fluorobis(pentafluorophenyl)borane diethyl etherate

: (Z)-3-(4-Dimethylamino-phenyl)-3-hydroxy-1-phenyl-propenone

: 1446682-13-8
bis(pentafluorophenyl)boron 1-[4-(dimethylamino)phenyl]-3-phenylpropane-1,3-dione

Guidance literature:: In tetrahydrofuran; for 12h; Reflux; Inert atmosphere;
DOI:10.1039/c5cc01113b

Reference yield: 58.0%

: 19743-33-0
4-(dimethylamino)dibenzoylmethane

: 1109-15-5
tris(pentafluorophenyl)borate

: 1446682-13-8
bis(pentafluorophenyl)boron 1-[4-(dimethylamino)phenyl]-3-phenylpropane-1,3-dione

Guidance literature:: In dichloromethane;
DOI:10.1016/j.tetlet.2013.05.099

Reference yield:

: 1202-25-1
methyl 4-(N,N-dimethylamino)benzoate

: 1446682-13-8
bis(pentafluorophenyl)boron 1-[4-(dimethylamino)phenyl]-3-phenylpropane-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 20 °C / Schlenk technique; Inert atmosphere

1.2: 8 h / Schlenk technique; Inert atmosphere; Reflux

2.1: dichloromethane

With sodium hydride; In tetrahydrofuran; dichloromethane; mineral oil; 1.1: |Claisen Condensation / 1.2: |Claisen Condensation;
DOI:10.1016/j.tetlet.2013.05.099