N-propargyl-N'-butyl-1,6,7,12-tetrakis(4-methyl-phenoxy)perylene-3,4:9,10-tetracarboxylic bisimide

Base Information

• Chemical Name: N-propargyl-N'-butyl-1,6,7,12-tetrakis(4-methyl-phenoxy)perylene-3,4:9,10-tetracarboxylic bisimide
• CAS No.: 924908-15-6
• Molecular Formula: C₅₉H₄₄N₂O₈
• Molecular Weight: 909.007

Synonyms:N-propargyl-N'-butyl-1,6,7,12-tetrakis(4-methyl-phenoxy)perylene-3,4:9,10-tetracarboxylic bisimide

Chemical Property of N-propargyl-N'-butyl-1,6,7,12-tetrakis(4-methyl-phenoxy)perylene-3,4:9,10-tetracarboxylic bisimide

Chemical Property:

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Technology Process of N-propargyl-N'-butyl-1,6,7,12-tetrakis(4-methyl-phenoxy)perylene-3,4:9,10-tetracarboxylic bisimide

There total 1 articles about N-propargyl-N'-butyl-1,6,7,12-tetrakis(4-methyl-phenoxy)perylene-3,4:9,10-tetracarboxylic bisimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

N-butyl-1,6,7,12-tetrakis(4-methylphenoxy)-3,4:9,10-perylene tetracarboxylic bisimide + propargyl bromide (106-96-7) → N-propargyl-N'-butyl-1,6,7,12-tetrakis(4-methyl-phenoxy)perylene-3,4:9,10-tetracarboxylic bisimide (924908-15-6)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; xylene; at 20 ℃; for 5.5h;

DOI:10.1246/cl.2006.1416

Reference yield: 20.0%

N-propargyl-N'-butyl-1,6,7,12-tetrakis(4-methyl-phenoxy)perylene-3,4:9,10-tetracarboxylic bisimide (924908-15-6) + 1,3,5-tris(4-bromophenyl)benzene (7511-49-1) → 1-[4'-{N'-butyl-1,6,7,12-tetrakis(4-methyl-phenoxy)perylene-3,4:9,10-tetracarboxylic bisimide-N-propargyl-yl}-phenyl-4-yl]-3,5-bis(4-bromophenyl)-benzene

Guidance literature:

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; triethylamine; triphenylphosphine; In N,N-dimethyl-formamide; at 70 ℃; for 6h;

DOI:10.1246/cl.2006.1416

Reference yield: 13.0%

N-propargyl-N'-butyl-1,6,7,12-tetrakis(4-methyl-phenoxy)perylene-3,4:9,10-tetracarboxylic bisimide (924908-15-6) + 1,3,5-tris(4-bromophenyl)benzene (7511-49-1) → 1,3-bis[4'-{N'-butyl-1,6,7,12-tetrakis(4-methyl-phenoxy)perylene-3,4:9,10-tetracarboxylic bisimide-N-propargyl-yl}-phenyl-4-yl]-5-(4-bromophenyl)-benzene

Guidance literature:

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; triethylamine; triphenylphosphine; In N,N-dimethyl-formamide; at 70 ℃; for 6h;

DOI:10.1246/cl.2006.1416

upstream raw materials:

propargyl bromide

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