Technology Process of C47H35N3
There total 3 articles about C47H35N3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
diethylamino-sulfur trifluoride;
In
dichloromethane;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: aluminum (III) chloride / dichloromethane / 5 h / -78 °C
2.1: caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / palladium diacetate / toluene / 100 °C
3.1: ethylmagnesium bromide / diethyl ether; dichloromethane / 0.75 h / 0 - 20 °C
3.2: 1.5 h / 0 - 20 °C
3.3: 0 °C
4.1: diethylamino-sulfur trifluoride / dichloromethane / 20 °C
With
aluminum (III) chloride; diethylamino-sulfur trifluoride; ethylmagnesium bromide; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl;
palladium diacetate;
In
diethyl ether; dichloromethane; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / palladium diacetate / toluene / 100 °C
2.1: ethylmagnesium bromide / diethyl ether; dichloromethane / 0.75 h / 0 - 20 °C
2.2: 1.5 h / 0 - 20 °C
2.3: 0 °C
3.1: diethylamino-sulfur trifluoride / dichloromethane / 20 °C
With
diethylamino-sulfur trifluoride; ethylmagnesium bromide; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl;
palladium diacetate;
In
diethyl ether; dichloromethane; toluene;
