2-(TRIFLUOROMETHYL)NAPHTO-[2,3-D]-IMIDAZOLE

Base Information

• Chemical Name: 2-(TRIFLUOROMETHYL)NAPHTO-[2,3-D]-IMIDAZOLE
• CAS No.: 30048-94-3
• Molecular Formula: C12H7 F3 N2
• Molecular Weight: 236.19
• Hs Code.: 2933990090
• Mol file: 30048-94-3.mol

Synonyms:2-(TRIFLUOROMETHYL)NAPHTO-[2,3-D]-IMIDAZOLE;2-(Trifluoromethyl)-1H-naphtho[2,3-d]imidazole

Chemical Property of 2-(TRIFLUOROMETHYL)NAPHTO-[2,3-D]-IMIDAZOLE

Chemical Property:

• PSA: 28.68000
• LogP: 3.73490

Purity/Quality:

99% ^*data from raw suppliers

2-(TRIFLUOROMETHYL)NAPHTO-[2,3-D]-IMIDAZOLE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(TRIFLUOROMETHYL)NAPHTO-[2,3-D]-IMIDAZOLE

There total 3 articles about 2-(TRIFLUOROMETHYL)NAPHTO-[2,3-D]-IMIDAZOLE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2,3-Diaminonaphthalene (771-97-1) + trifluoroacetic acid (76-05-1) → 2-(trifluoromethyl)-1H-naphtho[2,3-d]imidazole (30048-94-3)

Guidance literature:

at 70 ℃; for 16h;

DOI:10.1016/j.tetlet.2012.09.069

Reference yield: 73.0%

1,1,1,5,5,5-hexafluoroacetylacetone (1522-22-1) + 2,3-Diaminonaphthalene (771-97-1) → 2-(trifluoromethyl)-1H-naphtho[2,3-d]imidazole (30048-94-3)

Guidance literature:

With iron(III) trifluoromethanesulfonate; In N,N-dimethyl-formamide; at 80 ℃; for 24h;

DOI:10.1016/j.tetlet.2016.06.086

Reference yield:

→ 2-(trifluoromethyl)-1H-naphtho[2,3-d]imidazole (30048-94-3)

Guidance literature:

Aus 2,3-Diamino-naphthalin und CF3-COOH;

upstream raw materials:

2,3-Diaminonaphthalene

trifluoroacetic acid

1,1,1,5,5,5-hexafluoroacetylacetone