1,1'-(2-methoxy-1,3-phenylene)bis-2(1H)-pyrimidinone>

Base Information

Chemical Name:1,1'-(2-methoxy-1,3-phenylene)bis-2(1H)-pyrimidinone>
CAS No.:91084-78-5
Molecular Formula:C₃₃H₄₀N₄O₇
Molecular Weight:604.703
Hs Code.:

1,1'-(2-methoxy-1,3-phenylene)bis<tetrahydro-3-<2-methoxy-3-(hydroxymethyl)-5-methylphenyl>-2(1H)-pyrimidinone>

Synonyms:1,1'-(2-methoxy-1,3-phenylene)bis-2(1H)-pyrimidinone>

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Chemical Property of 1,1'-(2-methoxy-1,3-phenylene)bis-2(1H)-pyrimidinone>

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Technology Process of 1,1'-(2-methoxy-1,3-phenylene)bis-2(1H)-pyrimidinone>

There total 7 articles about 1,1'-(2-methoxy-1,3-phenylene)bis-2(1H)-pyrimidinone> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 129125-28-6
1,1'-(2-methoxy-1,3-phenylene)bis-2(1H)-pyrimidinone>

: 91084-78-5
1,1'-(2-methoxy-1,3-phenylene)bis-2(1H)-pyrimidinone>

Guidance literature:: With sodium hydrogencarbonate; In acetone; for 10h; Heating;

Reference yield: 38.0%

: 91110-52-0
1,1'-(2-methoxy-1,3-phenylene)bis-2(1H)-pyrimidinone>

: 77-78-1
dimethyl sulfate

: 91084-78-5
1,1'-(2-methoxy-1,3-phenylene)bis-2(1H)-pyrimidinone>

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; water; at 60 ℃; for 1h;
DOI:10.1021/ja00329a058

Reference yield:

: 129125-41-3
1,3-Diisocyanato-2-methoxy-benzene

: 91084-78-5
1,1'-(2-methoxy-1,3-phenylene)bis-2(1H)-pyrimidinone>

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / toluene / 3 h / 85 °C

2: 37 percent / NaOH, benzyltriethylammonium bromide / benzene; H₂O / 20 h / 50 °C

3: 90 percent / Dowex-50 sulfonic acid resin / methanol / 1.33 h

4: 38 percent / sodium hydroxide / tetrahydrofuran; H₂O / 1 h / 60 °C

With sodium hydroxide; Dowex-50 sulfonic acid resin; benzyltriethylammonium bromide; In tetrahydrofuran; methanol; water; toluene; benzene;
DOI:10.1021/ja00329a058