(4RS,4aRS,5SR,7SR,8RS,8aSR)-4,5,7-trimethyl-8-(benzyloxy)-4-(hydroxymethyl)-3,4,4a,5,6,7,8,8a-octahydronaphthalene

Base Information

Chemical Name:(4RS,4aRS,5SR,7SR,8RS,8aSR)-4,5,7-trimethyl-8-(benzyloxy)-4-(hydroxymethyl)-3,4,4a,5,6,7,8,8a-octahydronaphthalene
CAS No.:101032-69-3
Molecular Formula:C₂₁H₃₀O₂
Molecular Weight:314.468
Hs Code.:

Synonyms:(4RS,4aRS,5SR,7SR,8RS,8aSR)-4,5,7-trimethyl-8-(benzyloxy)-4-(hydroxymethyl)-3,4,4a,5,6,7,8,8a-octahydronaphthalene

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Chemical Property of (4RS,4aRS,5SR,7SR,8RS,8aSR)-4,5,7-trimethyl-8-(benzyloxy)-4-(hydroxymethyl)-3,4,4a,5,6,7,8,8a-octahydronaphthalene

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Technology Process of (4RS,4aRS,5SR,7SR,8RS,8aSR)-4,5,7-trimethyl-8-(benzyloxy)-4-(hydroxymethyl)-3,4,4a,5,6,7,8,8a-octahydronaphthalene

There total 1 articles about (4RS,4aRS,5SR,7SR,8RS,8aSR)-4,5,7-trimethyl-8-(benzyloxy)-4-(hydroxymethyl)-3,4,4a,5,6,7,8,8a-octahydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (1R,4aS,6S,8S,8aR)-5-Benzyloxy-1,6,8-trimethyl-1,2,4a,5,6,7,8,8a-octahydro-naphthalene-1-carbaldehyde

: 101032-69-3
(4RS,4aRS,5SR,7SR,8RS,8aSR)-4,5,7-trimethyl-8-(benzyloxy)-4-(hydroxymethyl)-3,4,4a,5,6,7,8,8a-octahydronaphthalene

: 101032-68-2
(4RS,4aRS,5SR,7SR,8SR,8aSR)-4,5,7-trimethyl-8-(benzyloxy)-4-(hydroxymethyl)-3,4,4a,5,6,7,8,8a-octahydronaphthalene

Guidance literature:: With diisobutylaluminium hydride; In diethyl ether; hexane; at -78 ℃; for 1h; Yield given. Yields of byproduct given;
DOI:10.1021/ja00238a030

Reference yield:

: 101032-69-3
(4RS,4aRS,5SR,7SR,8RS,8aSR)-4,5,7-trimethyl-8-(benzyloxy)-4-(hydroxymethyl)-3,4,4a,5,6,7,8,8a-octahydronaphthalene

: 101032-67-1
(4RS,4aRS,5SR,7SR,8RS,8aSR)-4,5,7-trimethyl-8-(benzyloxy)-3,4,4a,5,6,7,8,8a-octahydronaphthalene-4-carboxaldehyde

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; Yield given. Multistep reaction; 1) CH₂Cl₂, -60 deg C, 2) CH₂Cl₂, -60to -25 deg C;
DOI:10.1021/ja00238a030