N-(5-benzyl-4-phenyl-1,3-thiazol-2-yl)-4-(3-bromo-4-ethoxyphenyl)-4-oxobutanamide

Base Information

• Chemical Name: N-(5-benzyl-4-phenyl-1,3-thiazol-2-yl)-4-(3-bromo-4-ethoxyphenyl)-4-oxobutanamide
• CAS No.: 905589-62-0
• Molecular Formula: C₂₈H₂₅BrN₂O₃S
• Molecular Weight: 549.488

Synonyms:N-(5-benzyl-4-phenyl-1,3-thiazol-2-yl)-4-(3-bromo-4-ethoxyphenyl)-4-oxobutanamide

Chemical Property of N-(5-benzyl-4-phenyl-1,3-thiazol-2-yl)-4-(3-bromo-4-ethoxyphenyl)-4-oxobutanamide

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Technology Process of N-(5-benzyl-4-phenyl-1,3-thiazol-2-yl)-4-(3-bromo-4-ethoxyphenyl)-4-oxobutanamide

There total 1 articles about N-(5-benzyl-4-phenyl-1,3-thiazol-2-yl)-4-(3-bromo-4-ethoxyphenyl)-4-oxobutanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-phenyl-5-(phenylmethyl)-1,3-thiazol-2-amine (905592-30-5) + 4-(4-ethoxy-3-bromo-phenyl)-4-oxo-butyric acid (905590-14-9) → N-(5-benzyl-4-phenyl-1,3-thiazol-2-yl)-4-(3-bromo-4-ethoxyphenyl)-4-oxobutanamide (905589-62-0)

Guidance literature:

With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In acetonitrile; at 50 ℃; for 2h;

Reference yield:

N-(5-benzyl-4-phenyl-1,3-thiazol-2-yl)-4-(3-bromo-4-ethoxyphenyl)-4-oxobutanamide (905589-62-0) + ethyl acetate n-hexane + ethyl acrylate (140-88-5,9003-32-1) → (2E)-3-(5-{4-[(5-benzyl-4-phenyl-1,3-thiazol-2-yl)amino]-4-oxobutanoyl}-2-ethoxyphenyl)acrylic acid ethyl ester + ethyl (2E)-3-(5-14-[(5-benzyl-4-phenyl-1,3-thiazol-2-yl)amino]-4-oxobutanoyl}-2-ethoxyphenyl)acrylate

Guidance literature:

With triethylamine; triphenylphosphine; palladium diacetate; In water; N,N-dimethyl-formamide;

Reference yield:

N-(5-benzyl-4-phenyl-1,3-thiazol-2-yl)-4-(3-bromo-4-ethoxyphenyl)-4-oxobutanamide (905589-62-0) + ethyl acrylate (140-88-5,9003-32-1) → (2E)-3-(5-{4-[(5-benzyl-4-phenyl-1,3-thiazol-2-yl)amino]-4-oxobutanoyl}-2-ethoxyphenyl)acrylic acid ethyl ester

Guidance literature:

With triethylamine; triphenylphosphine; palladium diacetate; In N,N-dimethyl-formamide; at 100 ℃;

upstream raw materials:

4-phenyl-5-(phenylmethyl)-1,3-thiazol-2-amine

4-(4-ethoxy-3-bromo-phenyl)-4-oxo-butyric acid

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