2,6-dimethoxy-4-(3-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-5-yl)phenol

Base Information

• Chemical Name: 2,6-dimethoxy-4-(3-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-5-yl)phenol
• CAS No.: 1189742-26-4
• Molecular Formula: C₂₀H₂₃NO₇
• Molecular Weight: 389.405

Synonyms:2,6-dimethoxy-4-(3-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-5-yl)phenol

Chemical Property of 2,6-dimethoxy-4-(3-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-5-yl)phenol

Chemical Property:

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Technology Process of 2,6-dimethoxy-4-(3-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-5-yl)phenol

There total 1 articles about 2,6-dimethoxy-4-(3-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-5-yl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

5-(4-(tert-butyldimethylsilyloxy)-3,5-dimethoxyphenyl)-3-(3,4,5-trimethoxy-phenyl)-4,5-dihydroisoxazole (1246651-07-9) → 2,6-dimethoxy-4-(3-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-5-yl)phenol (1189742-26-4)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 2h;

DOI:10.1016/j.ejmech.2010.05.047

Reference yield: 80.0%

2,6-dimethoxy-4-(3-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-5-yl)phenol (1189742-26-4) + 2-(4-(5-bromopentyloxy)-3-methoxyphenyl)-2,3-dihydroquinazolin-4(1H)-one (1227741-07-2) → 2-[4-(5-{2,6-dimethoxy-4-[3-(3,4,5-trimethoxy-phenyl)-4,5-dihydro-isoxazol-5-yl]-phenoxy}-pentyloxy)-3-methoxy-phenyl]-2,3-dihydro-1H-quinazolin-4-one (1227738-53-5)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 30 ℃; for 30h;

Reference yield: 80.0%

2,6-dimethoxy-4-(3-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-5-yl)phenol (1189742-26-4) + (2S)-N-[4-(3-bromopropoxy)-5-methoxy-2-nitrobenzoyl]pyrrolidine-2-carboxaldehyde diethyl thioacetal (343308-55-4) → [(2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-pyrrol-1-yl]-[4-(3-{2,6-dimethoxy-4-[3-(3,4,5-trimethoxyphenyl)-4,5-dihydro-5-isoxazolyl]phenoxy}propoxy)-5-methoxy-2-nitrophenyl]methanone (1189742-36-6)

Guidance literature:

With potassium carbonate; In acetone; for 24h; Reflux;

upstream raw materials:

5-(4-(tert-butyldimethylsilyloxy)-3,5-dimethoxyphenyl)-3-(3,4,5-trimethoxy-phenyl)-4,5-dihydroisoxazole

Downstream raw materials:

[(2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-pyrrol-1-yl]-[4-(3-{2,6-dimethoxy-4-[3-(3,4,5-trimethoxyphenyl)-4,5-dihydro-5-isoxazolyl]phenoxy}propoxy)-5-methoxy-2-nitrophenyl]methanone

2-[4-(5-{2,6-dimethoxy-4-[3-(3,4,5-trimethoxy-phenyl)-4,5-dihydro-isoxazol-5-yl]-phenoxy}-pentyloxy)-3-methoxy-phenyl]-2,3-dihydro-1H-quinazolin-4-one

C₄₁H₅₃N₃O₁₂S₂

C₄₂H₅₅N₃O₁₂S₂

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