N-[2-(tert-butyldiphenylsilanyloxy)-ethyl]-2-chloro-5-nitro-benzenesulfonamide

Base Information

Chemical Name:N-[2-(tert-butyldiphenylsilanyloxy)-ethyl]-2-chloro-5-nitro-benzenesulfonamide
CAS No.:1159282-08-2
Molecular Formula:C₂₄H₂₇ClN₂O₅SSi
Molecular Weight:519.093
Hs Code.:

Synonyms:N-[2-(tert-butyldiphenylsilanyloxy)-ethyl]-2-chloro-5-nitro-benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[2-(tert-butyldiphenylsilanyloxy)-ethyl]-2-chloro-5-nitro-benzenesulfonamide

Chemical Property:

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Technology Process of N-[2-(tert-butyldiphenylsilanyloxy)-ethyl]-2-chloro-5-nitro-benzenesulfonamide

There total 1 articles about N-[2-(tert-butyldiphenylsilanyloxy)-ethyl]-2-chloro-5-nitro-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 91578-89-1
2-((tert-butyldiphenylsilyl)oxy)ethanamine

: 4533-95-3
5-nitro-2-chlorobenzenesulfonyl chloride

: 1159282-08-2
N-[2-(tert-butyldiphenylsilanyloxy)-ethyl]-2-chloro-5-nitro-benzenesulfonamide

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃;

Reference yield:

: 1159282-08-2
N-[2-(tert-butyldiphenylsilanyloxy)-ethyl]-2-chloro-5-nitro-benzenesulfonamide

: 129018-68-4
2-chloro-N-(2-hydroxyethyl)-5-nitrobenzenesulfonamide

Guidance literature:: N-[2-(tert-butyldiphenylsilanyloxy)-ethyl]-2-chloro-5-nitro-benzenesulfonamide; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 2h;

With water; sodium chloride; In tetrahydrofuran; ethyl acetate;

Reference yield:

: 1159282-08-2
N-[2-(tert-butyldiphenylsilanyloxy)-ethyl]-2-chloro-5-nitro-benzenesulfonamide

: 436095-41-9
3-amino-N-(2-hydroxyethyl)-benzenesulphonamide

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

2: hydrogen / palladium 10% on activated carbon / methanol / 750.08 Torr / Inert atmosphere

With tetrabutyl ammonium fluoride; hydrogen; palladium 10% on activated carbon; In tetrahydrofuran; methanol;