Technology Process of 3-deoxy-4,6-O-p-methoxybenzylidene-D-galactal
There total 3 articles about 3-deoxy-4,6-O-p-methoxybenzylidene-D-galactal which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium 1-naphthalenide;
In
tetrahydrofuran;
at -40 ℃;
DOI:10.1021/jo102382r
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.75 h / 0 - 20 °C
1.2: 16 h / 20 °C
2.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 0.5 h / Reflux
3.1: lithium 1-naphthalenide / tetrahydrofuran / -40 °C
With
2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium hydride; lithium 1-naphthalenide;
In
tetrahydrofuran; toluene; mineral oil;
DOI:10.1021/jo102382r
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 0.5 h / Reflux
2: lithium 1-naphthalenide / tetrahydrofuran / -40 °C
With
2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; lithium 1-naphthalenide;
In
tetrahydrofuran; toluene;
DOI:10.1021/jo102382r
