N-t-butoxycarbonyl-(4-fluoro-2-(methylthio)phenyl)methanamine

Base Information

• Chemical Name: N-t-butoxycarbonyl-(4-fluoro-2-(methylthio)phenyl)methanamine
• CAS No.: 869591-73-1
• Molecular Formula: C₁₃H₁₈FNO₂S
• Molecular Weight: 271.356
• Mol file: 869591-73-1.mol

Synonyms:N-t-butoxycarbonyl-(4-fluoro-2-(methylthio)phenyl)methanamine

Chemical Property of N-t-butoxycarbonyl-(4-fluoro-2-(methylthio)phenyl)methanamine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of N-t-butoxycarbonyl-(4-fluoro-2-(methylthio)phenyl)methanamine

There total 1 articles about N-t-butoxycarbonyl-(4-fluoro-2-(methylthio)phenyl)methanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-fluoro-2-(methylthio)benzylamine (410545-49-2) + di-tert-butyl dicarbonate (24424-99-5) → N-t-butoxycarbonyl-(4-fluoro-2-(methylthio)phenyl)methanamine (869591-73-1)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 0.5h;

Reference yield:

N-t-butoxycarbonyl-(4-fluoro-2-(methylthio)phenyl)methanamine (869591-73-1) → 4-fluoro-2-(methylsulfonyl)benzylamine hydrochloride

Guidance literature:

N-t-butoxycarbonyl-(4-fluoro-2-(methylthio)phenyl)methanamine; With Oxone; In acetone; at 60 ℃; for 1.5h;

With hydrogenchloride; In ethanol; at 60 ℃; for 2h;

Reference yield:

N-t-butoxycarbonyl-(4-fluoro-2-(methylthio)phenyl)methanamine (869591-73-1) → C13H18FNO4S (1214988-99-4)

Guidance literature:

With Oxone; In water; acetone; at 60 ℃; for 1.66667h;

upstream raw materials:

4-fluoro-2-(methylthio)benzylamine

di-tert-butyl dicarbonate

Downstream raw materials:

C₁₃H₁₈FNO₄S