2-formyl-7,8-dimethoxy-5-phenylsulfanyl-2,3,4,5-tetrahydro-1H-2-benzazepine

Base Information

Chemical Name:2-formyl-7,8-dimethoxy-5-phenylsulfanyl-2,3,4,5-tetrahydro-1H-2-benzazepine
CAS No.:341548-04-7
Molecular Formula:C₁₉H₂₁NO₃S
Molecular Weight:343.447
Hs Code.:

Synonyms:2-formyl-7,8-dimethoxy-5-phenylsulfanyl-2,3,4,5-tetrahydro-1H-2-benzazepine

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Chemical Property of 2-formyl-7,8-dimethoxy-5-phenylsulfanyl-2,3,4,5-tetrahydro-1H-2-benzazepine

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Technology Process of 2-formyl-7,8-dimethoxy-5-phenylsulfanyl-2,3,4,5-tetrahydro-1H-2-benzazepine

There total 6 articles about 2-formyl-7,8-dimethoxy-5-phenylsulfanyl-2,3,4,5-tetrahydro-1H-2-benzazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 341547-98-6
N-(3,4-dimethoxyphenyl)methyl-N-[(3-phenylsulfinyl)propyl]formamide

: 341548-04-7
2-formyl-7,8-dimethoxy-5-phenylsulfanyl-2,3,4,5-tetrahydro-1H-2-benzazepine

: 341547-92-0
N-(3,4-dimethoxyphenyl)methyl-N-[(3-phenylsulfanyl)propyl]formamide

Guidance literature:: With boron trifluoride diethyl etherate; trifluoroacetic anhydride; In benzene; at 20 ℃; for 1.5h;
DOI:10.3987/com-00-s(i)97

Reference yield: 31.0%

: 341547-98-6
N-(3,4-dimethoxyphenyl)methyl-N-[(3-phenylsulfinyl)propyl]formamide

: N-[(3,5-dimethoxyphenyl)methyl]-N-[(3-phenylsulfanyl)-2-propenyl]formamide

: 341548-04-7
2-formyl-7,8-dimethoxy-5-phenylsulfanyl-2,3,4,5-tetrahydro-1H-2-benzazepine

Guidance literature:: With trifluoroacetic anhydride; In benzene; at 20 ℃; for 4h;
DOI:10.3987/com-00-s(i)97

Reference yield:

: 2015-09-0
3-(phenylthio)propylamine

: 341548-04-7
2-formyl-7,8-dimethoxy-5-phenylsulfanyl-2,3,4,5-tetrahydro-1H-2-benzazepine

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid / ethanol / 23 h / Heating

1.2: 74 percent / NaBH₄ / ethanol / 0.5 h / 0 - 20 °C

2.1: 100 percent / Ac₂O / 1 h / 70 °C

3.1: 84 percent / NaIO₄ / H₂O; methanol / 5 h / 20 °C

4.1: 56 percent / TFAA / benzene / 4 h / 20 °C

With sodium periodate; acetic anhydride; acetic acid; trifluoroacetic anhydride; In methanol; ethanol; water; benzene;
DOI:10.3987/com-00-s(i)97