2-[1-(2,3-dimethyl-phenyl)-1H-tetrazol-5-ylsulfanyl]-N-[2-(4-methoxy-3-methyl-benzyl)-2H-pyrazol-3-yl]-acetamide

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Chemical Name:2-[1-(2,3-dimethyl-phenyl)-1H-tetrazol-5-ylsulfanyl]-N-[2-(4-methoxy-3-methyl-benzyl)-2H-pyrazol-3-yl]-acetamide
CAS No.:1200438-28-3
Molecular Formula:C₂₃H₂₅N₇O₂S
Molecular Weight:463.563
Hs Code.:

Synonyms:2-[1-(2,3-dimethyl-phenyl)-1H-tetrazol-5-ylsulfanyl]-N-[2-(4-methoxy-3-methyl-benzyl)-2H-pyrazol-3-yl]-acetamide

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Chemical Property of 2-[1-(2,3-dimethyl-phenyl)-1H-tetrazol-5-ylsulfanyl]-N-[2-(4-methoxy-3-methyl-benzyl)-2H-pyrazol-3-yl]-acetamide

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Technology Process of 2-[1-(2,3-dimethyl-phenyl)-1H-tetrazol-5-ylsulfanyl]-N-[2-(4-methoxy-3-methyl-benzyl)-2H-pyrazol-3-yl]-acetamide

There total 4 articles about 2-[1-(2,3-dimethyl-phenyl)-1H-tetrazol-5-ylsulfanyl]-N-[2-(4-methoxy-3-methyl-benzyl)-2H-pyrazol-3-yl]-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 436095-13-5
[1-(2,3-dimethyl-phenyl)-1H-tetrazol-5-ylsulfanyl]-acetic acid

: 1200439-86-6
2-(4-methoxy-3-methyl-benzyl)-2H-pyrazol-3-ylamine

: 1200438-28-3
2-[1-(2,3-dimethyl-phenyl)-1H-tetrazol-5-ylsulfanyl]-N-[2-(4-methoxy-3-methyl-benzyl)-2H-pyrazol-3-yl]-acetamide

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 18h;

Reference yield:

: 1200439-85-5
[1-(2,3-dimethyl-phenyl)-1H-tetrazol-5-ylsulfanyl]-acetic acid ethyl ester

: 1200438-28-3
2-[1-(2,3-dimethyl-phenyl)-1H-tetrazol-5-ylsulfanyl]-N-[2-(4-methoxy-3-methyl-benzyl)-2H-pyrazol-3-yl]-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide; water / water; tetrahydrofuran; methanol; aq. NaOH solution / 20 °C

1.2: pH 3

2.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 18 h / 20 °C

With dmap; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In tetrahydrofuran; methanol; aq. NaOH solution; water; N,N-dimethyl-formamide;

Reference yield:

: 851721-95-4
1-(2,3-dimethyl-phenyl)-1H-tetrazole-5-thiol

: 1200438-28-3
2-[1-(2,3-dimethyl-phenyl)-1H-tetrazol-5-ylsulfanyl]-N-[2-(4-methoxy-3-methyl-benzyl)-2H-pyrazol-3-yl]-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine / dimethyl sulfoxide / 2.5 h / 20 °C

2.1: sodium hydroxide; water / water; tetrahydrofuran; methanol; aq. NaOH solution / 20 °C

2.2: pH 3

3.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 18 h / 20 °C

With pyridine; dmap; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In tetrahydrofuran; methanol; aq. NaOH solution; water; dimethyl sulfoxide; N,N-dimethyl-formamide;