2-(chloromethyl)-5-((2,4-dimethoxybenzyl)amino)-7-cyano-[1,2,4]triazolo[1,5-c]quinazoline

Base Information

Chemical Name:2-(chloromethyl)-5-((2,4-dimethoxybenzyl)amino)-7-cyano-[1,2,4]triazolo[1,5-c]quinazoline
CAS No.:1616709-05-7
Molecular Formula:C₂₀H₁₇ClN₆O₂
Molecular Weight:408.847
Hs Code.:

Synonyms:2-(chloromethyl)-5-((2,4-dimethoxybenzyl)amino)-7-cyano-[1,2,4]triazolo[1,5-c]quinazoline

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Chemical Property of 2-(chloromethyl)-5-((2,4-dimethoxybenzyl)amino)-7-cyano-[1,2,4]triazolo[1,5-c]quinazoline

Chemical Property:

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Technology Process of 2-(chloromethyl)-5-((2,4-dimethoxybenzyl)amino)-7-cyano-[1,2,4]triazolo[1,5-c]quinazoline

There total 3 articles about 2-(chloromethyl)-5-((2,4-dimethoxybenzyl)amino)-7-cyano-[1,2,4]triazolo[1,5-c]quinazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1616709-07-9
C₂₁H₂₀N₆O₅S

: 1616709-05-7
2-(chloromethyl)-5-((2,4-dimethoxybenzyl)amino)-7-cyano-[1,2,4]triazolo[1,5-c]quinazoline

Guidance literature:: With lithium chloride; In acetone; at 58 ℃; for 3h;

Reference yield:

: 1616709-04-6
7-bromo-5-((2,4-dimethoxybenzyl)amino)-2-hydroxymethyl-[1,2,4]triazolo[1,5-c]quinazoline

: 1616709-05-7
2-(chloromethyl)-5-((2,4-dimethoxybenzyl)amino)-7-cyano-[1,2,4]triazolo[1,5-c]quinazoline

Guidance literature:: Multi-step reaction with 3 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / water; N,N-dimethyl-formamide / 14 h / 120 °C / Inert atmosphere

2: triethylamine / chloroform-d1; dichloromethane / 50 h / 20 °C / Cooling with ice

3: lithium chloride / acetone / 3 h / 58 °C

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triethylamine; lithium chloride; In chloroform-d1; dichloromethane; water; N,N-dimethyl-formamide; acetone;

Reference yield:

: 1616709-06-8
C₂₀H₁₈N₆O₃

: 1616709-05-7
2-(chloromethyl)-5-((2,4-dimethoxybenzyl)amino)-7-cyano-[1,2,4]triazolo[1,5-c]quinazoline

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / chloroform-d1; dichloromethane / 50 h / 20 °C / Cooling with ice

2: lithium chloride / acetone / 3 h / 58 °C

With triethylamine; lithium chloride; In chloroform-d1; dichloromethane; acetone;