C₂₁H₁₇ClFNO₃S

Base Information

Chemical Name:C₂₁H₁₇ClFNO₃S
CAS No.:1273308-67-0
Molecular Formula:C₂₁H₁₇ClFNO₃S
Molecular Weight:417.888
Hs Code.:

C<sub>21</sub>H<sub>17</sub>ClFNO<sub>3</sub>S

Synonyms:C₂₁H₁₇ClFNO₃S

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Chemical Property of C₂₁H₁₇ClFNO₃S

Chemical Property:

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Technology Process of C₂₁H₁₇ClFNO₃S

There total 9 articles about C₂₁H₁₇ClFNO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1273308-64-7
C₂₉H₂₃ClFNO₅S

: 1273308-67-0
C₂₁H₁₇ClFNO₃S

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In ethanol; dichloromethane; ethyl acetate; for 0.5h; under 760.051 Torr;

Reference yield:

: 69363-85-5
methyl 4-aminothiophene-3-carboxylate

: 1273308-67-0
C₂₁H₁₇ClFNO₃S

Guidance literature:: Multi-step reaction with 6 steps

1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 - 20 °C

2: N-Bromosuccinimide / acetonitrile

3: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 1 h / 80 °C / Inert atmosphere

4: hydrogen / palladium 10% on activated carbon / dichloromethane; ethyl acetate; ethanol / 4 h / 760.05 Torr

5: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 2.5 h / 20 °C

6: hydrogen / palladium 10% on activated carbon / dichloromethane; ethyl acetate; ethanol / 0.5 h / 760.05 Torr

With N-Bromosuccinimide; hydrogen; sodium carbonate; N-ethyl-N,N-diisopropylamine; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate; toluene; acetonitrile;

Reference yield:

: 150-30-1,25191-15-5,658-69-5,67675-33-6
Phenylalanine

: 1273308-67-0
C₂₁H₁₇ClFNO₃S

Guidance literature:: Multi-step reaction with 4 steps

1: sodium nitrite; pyridine hydrofluoride / 18 h / 20 °C

2: oxalyl dichloride / dmap / dichloromethane / 2 h / 20 °C

3: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 2.5 h / 20 °C

4: hydrogen / palladium 10% on activated carbon / dichloromethane; ethyl acetate; ethanol / 0.5 h / 760.05 Torr

With oxalyl dichloride; pyridine hydrofluoride; hydrogen; N-ethyl-N,N-diisopropylamine; sodium nitrite; dmap; palladium 10% on activated carbon; In ethanol; dichloromethane; ethyl acetate;