C₂₆H₂₃N₃O₃

Base Information

Chemical Name:C₂₆H₂₃N₃O₃
CAS No.:1360445-24-4
Molecular Formula:C₂₆H₂₃N₃O₃
Molecular Weight:425.487
Hs Code.:

C<sub>26</sub>H<sub>23</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:C₂₆H₂₃N₃O₃

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Chemical Property of C₂₆H₂₃N₃O₃

Chemical Property:

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Technology Process of C₂₆H₂₃N₃O₃

There total 3 articles about C₂₆H₂₃N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1360445-01-7
C₁₇H₁₄BrN₃O₂

: 1360445-24-4
C₂₆H₂₃N₃O₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: boron dimethyl-trifluoro sulphide / dichloromethane; 1,2-dichloro-ethane / Reflux; Inert atmosphere

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane / 0.67 h / 20 °C / Inert atmosphere

2.2: 16 h / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; boron dimethyl-trifluoro sulphide; In 1,2-dimethoxyethane; dichloromethane; 1,2-dichloro-ethane; 2.2: Suzuki-Miyaura coupling;
DOI:10.1016/j.bmcl.2011.12.015

Reference yield:

: 78725-40-3
C₁₀H₇BrO₂

: 1360445-24-4
C₂₆H₂₃N₃O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium azide / water / 24 h / 100 °C / Inert atmosphere

2.1: boron dimethyl-trifluoro sulphide / dichloromethane; 1,2-dichloro-ethane / Reflux; Inert atmosphere

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane / 0.67 h / 20 °C / Inert atmosphere

3.2: 16 h / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium azide; boron dimethyl-trifluoro sulphide; In 1,2-dimethoxyethane; dichloromethane; water; 1,2-dichloro-ethane; 3.2: Suzuki-Miyaura coupling;
DOI:10.1016/j.bmcl.2011.12.015

Reference yield:

: 1761-61-1
5-bromosalicyclaldehyde

: 1360445-24-4
C₂₆H₂₃N₃O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium carbonate / acetone / 8 h / Inert atmosphere; Reflux

2.1: tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3.1: Jones reagent / acetone / 0.5 h / 0 °C / Inert atmosphere

4.1: sodium azide / water / 24 h / 100 °C / Inert atmosphere

5.1: boron dimethyl-trifluoro sulphide / dichloromethane; 1,2-dichloro-ethane / Reflux; Inert atmosphere

6.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane / 0.67 h / 20 °C / Inert atmosphere

6.2: 16 h / Inert atmosphere; Reflux

With Jones reagent; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium azide; boron dimethyl-trifluoro sulphide; sodium carbonate; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; 1,2-dichloro-ethane; acetone; 6.2: Suzuki-Miyaura coupling;
DOI:10.1016/j.bmcl.2011.12.015