6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl 3,4,6-tri-O-acetyl-2-O-benzoyl-β-D-mannopyranosyl-(1->4)-[2,3,4-tri-O-acetyl-α-L-fucopyranosyl-(1->3)]-2-O-benzoyl-6-O-acetyl-β-D-glucopyranoside

Base Information Edit

Chemical Name:6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl 3,4,6-tri-O-acetyl-2-O-benzoyl-β-D-mannopyranosyl-(1->4)-[2,3,4-tri-O-acetyl-α-L-fucopyranosyl-(1->3)]-2-O-benzoyl-6-O-acetyl-β-D-glucopyranoside
CAS No.:904319-37-5
Molecular Formula:C₅₅H₆₈Cl₃NO₂₆
Molecular Weight:1265.5
Hs Code.:
Mol file:904319-37-5.mol

6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl 3,4,6-tri-O-acetyl-2-O-benzoyl-β-D-mannopyranosyl-(1->4)-[2,3,4-tri-O-acetyl-α-L-fucopyranosyl-(1->3)]-2-O-benzoyl-6-O-acetyl-β-D-glucopyranoside

Synonyms:6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl 3,4,6-tri-O-acetyl-2-O-benzoyl-β-D-mannopyranosyl-(1->4)-[2,3,4-tri-O-acetyl-α-L-fucopyranosyl-(1->3)]-2-O-benzoyl-6-O-acetyl-β-D-glucopyranoside

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Chemical Property of 6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl 3,4,6-tri-O-acetyl-2-O-benzoyl-β-D-mannopyranosyl-(1->4)-[2,3,4-tri-O-acetyl-α-L-fucopyranosyl-(1->3)]-2-O-benzoyl-6-O-acetyl-β-D-glucopyranoside Edit

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Technology Process of 6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl 3,4,6-tri-O-acetyl-2-O-benzoyl-β-D-mannopyranosyl-(1->4)-[2,3,4-tri-O-acetyl-α-L-fucopyranosyl-(1->3)]-2-O-benzoyl-6-O-acetyl-β-D-glucopyranoside

There total 2 articles about 6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl 3,4,6-tri-O-acetyl-2-O-benzoyl-β-D-mannopyranosyl-(1->4)-[2,3,4-tri-O-acetyl-α-L-fucopyranosyl-(1->3)]-2-O-benzoyl-6-O-acetyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 904319-34-2
2-(trimethylsilyl)ethyl 3,4,6-tri-O-acetyl-2-O-benzoyl-β-D-mannopyranosyl-(1->4)-[2,3,4-tri-O-acetyl-α-L-fucopyranosyl-(1->3)]-2-O-benzoyl-6-O-acetyl-β-D-glucopyranoside

: 904319-37-5
6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl 3,4,6-tri-O-acetyl-2-O-benzoyl-β-D-mannopyranosyl-(1->4)-[2,3,4-tri-O-acetyl-α-L-fucopyranosyl-(1->3)]-2-O-benzoyl-6-O-acetyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: CF₃CO₂H / CH₂Cl₂ / 2.5 h / 0 - 20 °C

1.2: 86 percent / DBU / CH₂Cl₂ / 2 h / 0 °C

2.1: 100 percent / AW₃₀₀ molecular sieves; TMSOTf / CH₂Cl₂ / 4 h / 0 °C

With molecular sieve; trimethylsilyl trifluoromethanesulfonate; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.carres.2006.04.019

Reference yield:

: 4048-33-3
6-amino-1-hexanol

: 904319-37-5
6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl 3,4,6-tri-O-acetyl-2-O-benzoyl-β-D-mannopyranosyl-(1->4)-[2,3,4-tri-O-acetyl-α-L-fucopyranosyl-(1->3)]-2-O-benzoyl-6-O-acetyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / MgO / dioxane; H₂O / 16 h / 20 °C

2: 100 percent / AW₃₀₀ molecular sieves; TMSOTf / CH₂Cl₂ / 4 h / 0 °C

With molecular sieve; trimethylsilyl trifluoromethanesulfonate; magnesium oxide; In 1,4-dioxane; dichloromethane; water;
DOI:10.1016/j.carres.2006.04.019