C₃₄H₄₇N₉O₁₀

Base Information

Chemical Name:C₃₄H₄₇N₉O₁₀
CAS No.:175695-28-0
Molecular Formula:C₃₄H₄₇N₉O₁₀
Molecular Weight:741.801
Hs Code.:

C<sub>34</sub>H<sub>47</sub>N<sub>9</sub>O<sub>10</sub>

Synonyms:C₃₄H₄₇N₉O₁₀

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₄H₄₇N₉O₁₀

Chemical Property:

Purity/Quality:

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Technology Process of C₃₄H₄₇N₉O₁₀

There total 6 articles about C₃₄H₄₇N₉O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23124-10-9
2-(N₉-adeninyl)acetic acid methyl ester

: 175695-28-0
C₃₄H₄₇N₉O₁₀

Guidance literature:: Multi-step reaction with 5 steps

1: 57 percent / DMAP / dimethylformamide

2: 83 percent / LiOH / dioxane; H₂O

3: 1.) triphenyl phosphine, N-bromosucciniomide; 2.) N-methylmorpholine / 1.) CH₂Cl₂

4: 100 percent / tetrakis(triphenyl phosphine)palladium, morpholine / tetrahydrofuran

5: 1.) DCC, HOSu; 2.) NMM / 1.) CH₂Cl₂, 18 h; 2.) -15 degC

With morpholine; 4-methyl-morpholine; dmap; lithium hydroxide; 1-hydroxy-pyrrolidine-2,5-dione; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dicyclohexyl-carbodiimide; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1016/0040-4039(96)00037-8

Reference yield:

: 66224-66-6,66224-67-7,66224-68-8,66224-69-9,134434-48-3,134434-49-4,134454-76-5,134461-75-9
adenine

: 175695-28-0
C₃₄H₄₇N₉O₁₀

Guidance literature:: Multi-step reaction with 6 steps

1: 90 percent / NaH / dimethylformamide

2: 57 percent / DMAP / dimethylformamide

3: 83 percent / LiOH / dioxane; H₂O

4: 1.) triphenyl phosphine, N-bromosucciniomide; 2.) N-methylmorpholine / 1.) CH₂Cl₂

5: 100 percent / tetrakis(triphenyl phosphine)palladium, morpholine / tetrahydrofuran

6: 1.) DCC, HOSu; 2.) NMM / 1.) CH₂Cl₂, 18 h; 2.) -15 degC

With morpholine; 4-methyl-morpholine; dmap; lithium hydroxide; 1-hydroxy-pyrrolidine-2,5-dione; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydride; dicyclohexyl-carbodiimide; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1016/0040-4039(96)00037-8

Reference yield:

: 175695-25-7
ethyl [N⁶,N⁶-bis(tert-butoxycarbonyl)adenin-9-yl]acetic acid

: 175695-28-0
C₃₄H₄₇N₉O₁₀

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) triphenyl phosphine, N-bromosucciniomide; 2.) N-methylmorpholine / 1.) CH₂Cl₂

2: 100 percent / tetrakis(triphenyl phosphine)palladium, morpholine / tetrahydrofuran

3: 1.) DCC, HOSu; 2.) NMM / 1.) CH₂Cl₂, 18 h; 2.) -15 degC

With morpholine; 4-methyl-morpholine; 1-hydroxy-pyrrolidine-2,5-dione; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dicyclohexyl-carbodiimide; triphenylphosphine; In tetrahydrofuran;
DOI:10.1016/0040-4039(96)00037-8