{Mo(CO)2(PPh₃)(`buS₄')}

Base Information

Chemical Name:{Mo(CO)2(PPh₃)(`buS₄')}
CAS No.:135823-52-8
Molecular Formula:C₅₀H₅₉MoO₂PS₄
Molecular Weight:947.195
Hs Code.:

{Mo(CO)2(PPh<sub>3</sub>)(`buS<sub>4</sub>')}

Synonyms:{Mo(CO)2(PPh₃)(`buS₄')}

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {Mo(CO)2(PPh₃)(`buS₄')}

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Technology Process of {Mo(CO)2(PPh₃)(`buS₄')}

There total 1 articles about {Mo(CO)2(PPh₃)(`buS₄')} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: (1,2-bis(3,5-di(t-butyl)-2-mercaptophenylthio)ethane)-Li₂

: 82443-48-9,17250-39-4
{Mo(CO)3(P(C₆H₅)3)2(Cl)2}

: 135823-52-8
{Mo(CO)2(PPh₃)(`buS₄')}

Guidance literature:: With n-butyllithium; In methanol; addn. of Li-compd. to yellow suspension of (Mo(CO)3(PPh3)2(Cl)2)in MeOH under exclusion of light; under N2 in abs. solvents;; filtration after 14h at room temp., washing with MeOH and n-hexane and drying in vac.; elem. anal.;;
DOI:10.1016/0022-328X(91)80137-9

Reference yield: 44.0%

: 135823-52-8
{Mo(CO)2(PPh₃)(`buS₄')}

: 135823-51-7
molybdenum(IV)(carbonyl)(PPh₃)(3,5-di-t-butyl-1,2-benzenedithiolate)2

Guidance literature:: In tetrahydrofuran; byproducts: CO, C2H4; (N2); refluxing for 75 min;; evapn. to dryness; drying in vac. for 12 h; dissolving in CH2Cl2; filtration through SiO2; filtrate evapn. to dryness; recrystn. (CH2Cl2/MeOH); washing (MeOH, n-hexane); drying in vac.; elem. anal.;
DOI:10.1016/S0020-1693(00)83846-3

Reference yield:

: 135823-52-8
{Mo(CO)2(PPh₃)(`buS₄')}

: molybdenum(IV)(carbonyl)(PPh₃)(3,5-di-t-butyl-1,2-benzenedithiolate)2

Guidance literature:: In chloroform-d1; byproducts: CO, C2H4; (N2); room temp.; not isolated; detected by (1)H-; (13)C-; (31)P-NMR;
DOI:10.1016/S0020-1693(00)83846-3