(4Z,7Z,9E,11E)-(13R,14S)-13-((R)-2-Acetylamino-2-methoxycarbonyl-ethylsulfanyl)-14-hydroxy-octadeca-4,7,9,11-tetraenedioic acid 18-ethyl ester 1-methyl ester

Base Information

• Chemical Name: (4Z,7Z,9E,11E)-(13R,14S)-13-((R)-2-Acetylamino-2-methoxycarbonyl-ethylsulfanyl)-14-hydroxy-octadeca-4,7,9,11-tetraenedioic acid 18-ethyl ester 1-methyl ester
• CAS No.: 118884-88-1
• Molecular Formula: C₂₇H₄₁NO₈S
• Molecular Weight: 539.69

Synonyms:(4Z,7Z,9E,11E)-(13R,14S)-13-((R)-2-Acetylamino-2-methoxycarbonyl-ethylsulfanyl)-14-hydroxy-octadeca-4,7,9,11-tetraenedioic acid 18-ethyl ester 1-methyl ester

Chemical Property of (4Z,7Z,9E,11E)-(13R,14S)-13-((R)-2-Acetylamino-2-methoxycarbonyl-ethylsulfanyl)-14-hydroxy-octadeca-4,7,9,11-tetraenedioic acid 18-ethyl ester 1-methyl ester

Chemical Property:

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Technology Process of (4Z,7Z,9E,11E)-(13R,14S)-13-((R)-2-Acetylamino-2-methoxycarbonyl-ethylsulfanyl)-14-hydroxy-octadeca-4,7,9,11-tetraenedioic acid 18-ethyl ester 1-methyl ester

There total 1 articles about (4Z,7Z,9E,11E)-(13R,14S)-13-((R)-2-Acetylamino-2-methoxycarbonyl-ethylsulfanyl)-14-hydroxy-octadeca-4,7,9,11-tetraenedioic acid 18-ethyl ester 1-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

Ac-Cys-OMe (7652-46-2) + (4Z,7Z,9E,11E)-12-[(2S,3S)-3-(3-Ethoxycarbonyl-propyl)-oxiranyl]-dodeca-4,7,9,11-tetraenoic acid methyl ester (118884-86-9) → (4Z,7Z,9E,11E)-(13R,14S)-13-((R)-2-Acetylamino-2-methoxycarbonyl-ethylsulfanyl)-14-hydroxy-octadeca-4,7,9,11-tetraenedioic acid 18-ethyl ester 1-methyl ester (118884-88-1)

Guidance literature:

With TEMPOL; In methanol; triethylamine; for 3h; Ambient temperature;

DOI:10.1021/jo00276a025

Reference yield: 56.0%

(4Z,7Z,9E,11E)-(13R,14S)-13-((R)-2-Acetylamino-2-methoxycarbonyl-ethylsulfanyl)-14-hydroxy-octadeca-4,7,9,11-tetraenedioic acid 18-ethyl ester 1-methyl ester (118884-88-1) → 18-carboxy-19,20-dinor-N-acetyl-leukotriene E4 (114115-51-4)

Guidance literature:

With potassium carbonate; In methanol; Ambient temperature;

DOI:10.1021/jo00276a025

upstream raw materials:

Ac-Cys-OMe

(4Z,7Z,9E,11E)-12-[(2S,3S)-3-(3-Ethoxycarbonyl-propyl)-oxiranyl]-dodeca-4,7,9,11-tetraenoic acid methyl ester

Downstream raw materials:

18-carboxy-19,20-dinor-N-acetyl-leukotriene E₄

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