C₁₄H₁₇NO₆S

Base Information

Chemical Name:C₁₄H₁₇NO₆S
CAS No.:1432131-05-9
Molecular Formula:C₁₄H₁₇NO₆S
Molecular Weight:327.358
Hs Code.:

C<sub>14</sub>H<sub>17</sub>NO<sub>6</sub>S

Synonyms:C₁₄H₁₇NO₆S

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Chemical Property of C₁₄H₁₇NO₆S

Chemical Property:

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Technology Process of C₁₄H₁₇NO₆S

There total 3 articles about C₁₄H₁₇NO₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1432131-02-6
C₁₃H₁₅NO₃

: 1132-17-8
4-ethoxybenzenesulphonyl chloride

: 1432131-05-9
C₁₄H₁₇NO₆S

Guidance literature:: C₁₃H₁₅NO₃; With 10 wt% Pd(OH)2 on carbon; hydrogen; In ethanol; for 21.5h;

4-ethoxybenzenesulphonyl chloride; With triethylamine; In dichloromethane; at 20 ℃; for 2h; Cooling with ice;

Reference yield:

: 1432131-00-4
C₁₃H₁₃NO₃

: 1432131-05-9
C₁₄H₁₇NO₆S

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tetrahydroborate / methanol / 5.5 h / -78 °C

2.1: 10 wt% Pd(OH)2 on carbon; hydrogen / ethanol / 21.5 h

2.2: 2 h / 20 °C / Cooling with ice

With sodium tetrahydroborate; 10 wt% Pd(OH)2 on carbon; hydrogen; In methanol; ethanol;

Reference yield:

: 1432130-98-7
C₁₄H₁₇NO₄

: 1432131-05-9
C₁₄H₁₇NO₆S

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium tert-butylate / tetrahydrofuran; toluene / 0.33 h / 0 °C / Cooling with ice

2.1: sodium tetrahydroborate / methanol / 5.5 h / -78 °C

3.1: 10 wt% Pd(OH)2 on carbon; hydrogen / ethanol / 21.5 h

3.2: 2 h / 20 °C / Cooling with ice

With sodium tetrahydroborate; 10 wt% Pd(OH)2 on carbon; potassium tert-butylate; hydrogen; In tetrahydrofuran; methanol; ethanol; toluene;