(2S)-2-(((4-phenylpropyl)hydroxyphosphoryl)oxy)penatnoic acid benzyl ester

Base Information

Chemical Name:(2S)-2-(((4-phenylpropyl)hydroxyphosphoryl)oxy)penatnoic acid benzyl ester
CAS No.:152830-12-1
Molecular Formula:C₂₁H₂₇O₅P
Molecular Weight:390.416
Hs Code.:

Synonyms:(2S)-2-(((4-phenylpropyl)hydroxyphosphoryl)oxy)penatnoic acid benzyl ester

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Chemical Property of (2S)-2-(((4-phenylpropyl)hydroxyphosphoryl)oxy)penatnoic acid benzyl ester

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Technology Process of (2S)-2-(((4-phenylpropyl)hydroxyphosphoryl)oxy)penatnoic acid benzyl ester

There total 4 articles about (2S)-2-(((4-phenylpropyl)hydroxyphosphoryl)oxy)penatnoic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (S)-2-(3-Phenyl-propylphosphinoyloxy)-pentanoic acid benzyl ester

: 152830-12-1
(2S)-2-(((4-phenylpropyl)hydroxyphosphoryl)oxy)penatnoic acid benzyl ester

Guidance literature:: With sodium periodate; In 1,4-dioxane; water; for 3h; Ambient temperature;
DOI:10.1021/jm00030a008

Reference yield:

: 6600-40-4,498-18-0
L-Norvaline

: 152830-12-1
(2S)-2-(((4-phenylpropyl)hydroxyphosphoryl)oxy)penatnoic acid benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 1 N H₂SO₄, NaNO₂ / H₂O / 2 h / 0 °C

2: K₂CO₃ / dimethylformamide / 14 h / Ambient temperature

3: N,N'-dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / tetrahydrofuran / 2 h / 0 °C

4: NaIO₄ / dioxane; H₂O / 3 h / Ambient temperature

With dmap; sodium periodate; sulfuric acid; potassium carbonate; dicyclohexyl-carbodiimide; sodium nitrite; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00030a008

Reference yield:

: 41014-93-1,6450-97-1
2-(S)-hydroxyvaleric acid

: 152830-12-1
(2S)-2-(((4-phenylpropyl)hydroxyphosphoryl)oxy)penatnoic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / dimethylformamide / 14 h / Ambient temperature

2: N,N'-dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / tetrahydrofuran / 2 h / 0 °C

3: NaIO₄ / dioxane; H₂O / 3 h / Ambient temperature

With dmap; sodium periodate; potassium carbonate; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00030a008