{(iridium)2diiodo(carbonyl)2(μ-dioxo)(bis(diphenylphosphino)methane)}

Base Information

Chemical Name:{(iridium)2diiodo(carbonyl)2(μ-dioxo)(bis(diphenylphosphino)methane)}
CAS No.:130495-84-0
Molecular Formula:C₅₂H₄₄I₂Ir₂O₄P₄
Molecular Weight:1495.06
Hs Code.:

Synonyms:{(iridium)2diiodo(carbonyl)2(μ-dioxo)(bis(diphenylphosphino)methane)}

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Chemical Property of {(iridium)2diiodo(carbonyl)2(μ-dioxo)(bis(diphenylphosphino)methane)}

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Technology Process of {(iridium)2diiodo(carbonyl)2(μ-dioxo)(bis(diphenylphosphino)methane)}

There total 2 articles about {(iridium)2diiodo(carbonyl)2(μ-dioxo)(bis(diphenylphosphino)methane)} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: diiodo(μ-carbonyl)carbonylbis(bis(diphenylphosphino)methane)diiridium

: 130495-84-0
{(iridium)2diiodo(carbonyl)2(μ-dioxo)(bis(diphenylphosphino)methane)}

Guidance literature:: With air; In dichloromethane; standard Schlenk procedure; soln. of the iridium-compd. is stirred in a flask open to air for several hours; the red-orange soln. is transferred to another flask, while the purple solid is washed with CH2Cl2 and the washings added to the mother liquor, the soln. is stirred for several hours and solid is collected, process is repeated several times; elem. anal.;

Reference yield:

: diiodo(μ-carbonyl)carbonylbis(bis(diphenylphosphino)methane)diiridium

: 80937-33-3
oxygen

: 130495-84-0
{(iridium)2diiodo(carbonyl)2(μ-dioxo)(bis(diphenylphosphino)methane)}

Guidance literature:: In dichloromethane; dioxygen is passed through the soln.; elem. anal.;

Reference yield: 95.0%

: 130495-84-0
{(iridium)2diiodo(carbonyl)2(μ-dioxo)(bis(diphenylphosphino)methane)}

: 149560-77-0
{(iridium)2diiodo(carbonyl)2(μ-SO4)(bis(diphenylphosphino)methane)}*methylenedichloride

Guidance literature:: With SO₂; In dichloromethane; standard Schlenk procedure; SO2 is passed through a soln. of the iridium-compd., soln. is stirred for 0.5 h; soln. is concentrated, followed by addn. of Et2O, pptn.; elem. anal.;