C₁₅H₁₅NO

Base Information

Chemical Name:C₁₅H₁₅NO
CAS No.:1421845-48-8
Molecular Formula:C₁₅H₁₅NO
Molecular Weight:225.29
Hs Code.:

Synonyms:C₁₅H₁₅NO

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₁₅NO

Chemical Property:

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Technology Process of C₁₅H₁₅NO

There total 3 articles about C₁₅H₁₅NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52034-22-7
3-anilinocyclohexene

: 471-25-0
Propiolic acid

: 1421845-48-8
C₁₅H₁₅NO

Guidance literature:: Propiolic acid; With dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere;

3-anilinocyclohexene; In dichloromethane; at 0 - 20 ℃; for 25.5h; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.11.067

Reference yield:

: 62-53-3
aniline

: 1421845-48-8
C₁₅H₁₅NO

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetonitrile / 12.17 h / 0 - 20 °C

2.1: dicyclohexyl-carbodiimide / dichloromethane / 1 h / 0 °C / Inert atmosphere

2.2: 25.5 h / 0 - 20 °C / Inert atmosphere

With potassium carbonate; dicyclohexyl-carbodiimide; In dichloromethane; acetonitrile;
DOI:10.1016/j.tetlet.2012.11.067

Reference yield:

: 1541-25-9
3-amino-1-cyclohexene

: 1421845-48-8
C₁₅H₁₅NO

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetonitrile / 12.17 h / 0 - 20 °C

2.1: dicyclohexyl-carbodiimide / dichloromethane / 1 h / 0 °C / Inert atmosphere

2.2: 25.5 h / 0 - 20 °C / Inert atmosphere

With potassium carbonate; dicyclohexyl-carbodiimide; In dichloromethane; acetonitrile;
DOI:10.1016/j.tetlet.2012.11.067