C₅₂H₅₈

Base Information

Chemical Name:C₅₂H₅₈
CAS No.:1427698-07-4
Molecular Formula:C₅₂H₅₈
Molecular Weight:683.033
Hs Code.:

Synonyms:C₅₂H₅₈

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₂H₅₈

Chemical Property:

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Technology Process of C₅₂H₅₈

There total 5 articles about C₅₂H₅₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 591-50-4
iodobenzene

: 1403992-22-2
C₄₀H₅₀

: 1427698-07-4
C₅₂H₅₈

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diisopropylamine; In toluene; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/anie.201206964

Reference yield:

: 63262-06-6
1,4-dibromo-2,5-diiodobenzene

: 1427698-07-4
C₅₂H₅₈

Guidance literature:: Multi-step reaction with 4 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / toluene / 20 h / 20 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / toluene; water / 18 h / 100 °C / Inert atmosphere

3: potassium carbonate / methanol; dichloromethane / 2 h / 45 °C

4: diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / toluene / 2 h / 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; diisopropylamine; In methanol; dichloromethane; water; toluene;
DOI:10.1002/anie.201206964

Reference yield:

: 106-37-6
1.4-dibromobenzene

: 1427698-07-4
C₅₂H₅₈

Guidance literature:: Multi-step reaction with 5 steps

1: iodine; sulfuric acid / 24 h / 130 °C

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / toluene / 20 h / 20 °C / Inert atmosphere

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / toluene; water / 18 h / 100 °C / Inert atmosphere

4: potassium carbonate / methanol; dichloromethane / 2 h / 45 °C

5: diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / toluene / 2 h / 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; iodine; potassium carbonate; diisopropylamine; In methanol; dichloromethane; water; toluene;
DOI:10.1002/anie.201206964