NiCl₂{2-(diphenylphosphino)-N-((1-methyl-1H-imidazol-2-yl)methylene)ethanamine}

Base Information

Chemical Name:NiCl₂{2-(diphenylphosphino)-N-((1-methyl-1H-imidazol-2-yl)methylene)ethanamine}
CAS No.:1403229-48-0
Molecular Formula:C₁₉H₂₀Cl₂N₃NiP
Molecular Weight:450.958
Hs Code.:

NiCl<sub>2</sub>{2-(diphenylphosphino)-N-((1-methyl-1H-imidazol-2-yl)methylene)ethanamine}

Synonyms:NiCl₂{2-(diphenylphosphino)-N-((1-methyl-1H-imidazol-2-yl)methylene)ethanamine}

Suppliers and Price of NiCl₂{2-(diphenylphosphino)-N-((1-methyl-1H-imidazol-2-yl)methylene)ethanamine}

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of NiCl₂{2-(diphenylphosphino)-N-((1-methyl-1H-imidazol-2-yl)methylene)ethanamine}

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Technology Process of NiCl₂{2-(diphenylphosphino)-N-((1-methyl-1H-imidazol-2-yl)methylene)ethanamine}

There total 2 articles about NiCl₂{2-(diphenylphosphino)-N-((1-methyl-1H-imidazol-2-yl)methylene)ethanamine} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 29046-78-4
(1,2-dimethoxyethane)dichloronickel(II)

: 1402935-62-9
2-(diphenylphosphino)-N-((1-methyl-1H-imidazol-2-yl)methylene) ethanamine

: 1403229-48-0
NiCl₂{2-(diphenylphosphino)-N-((1-methyl-1H-imidazol-2-yl)methylene)ethanamine}

Guidance literature:: In dichloromethane; at 20 ℃; for 12h; Schlenk technique; Inert atmosphere;
DOI:10.1016/j.jorganchem.2012.07.044

Reference yield:

: 4848-43-5
(2-aminoethyl)diphenylphosphane

: 13750-81-7
N-methyl-2-imidazolcarboxaldehyde

: 1403229-48-0
NiCl₂{2-(diphenylphosphino)-N-((1-methyl-1H-imidazol-2-yl)methylene)ethanamine}

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 20 °C / Schlenk technique; Inert atmosphere

2: dichloromethane / 12 h / 20 °C / Schlenk technique; Inert atmosphere

In dichloromethane;
DOI:10.1016/j.jorganchem.2012.07.044