Technology Process of C74H74O11
There total 5 articles about C74H74O11 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
1-(4'-hydroxyphenyl)-1,2,2-triphenylethylene;
With
potassium carbonate;
In
acetonitrile;
at 20 ℃;
for 0.5h;
C48H55BrO10;
With
potassium iodide;
In
acetonitrile;
for 40h;
Reflux;
Inert atmosphere;
DOI:10.1039/c4cc03105a
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: phosphorus trichloride; phosphoric acid; zinc(II) chloride
2.1: titanium tetrachloride; zinc / tetrahydrofuran / 0 °C / Reflux; Inert atmosphere
3.1: potassium carbonate / acetonitrile / 0.5 h / 20 °C
3.2: 40 h / Reflux; Inert atmosphere
With
phosphoric acid; titanium tetrachloride; potassium carbonate; zinc(II) chloride; zinc; phosphorus trichloride;
In
tetrahydrofuran; acetonitrile;
2.1: |McMurry Reaction;
DOI:10.1039/c4cc03105a
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: phosphorus trichloride; phosphoric acid; zinc(II) chloride
2.1: titanium tetrachloride; zinc / tetrahydrofuran / 0 °C / Reflux; Inert atmosphere
3.1: potassium carbonate / acetonitrile / 0.5 h / 20 °C
3.2: 40 h / Reflux; Inert atmosphere
With
phosphoric acid; titanium tetrachloride; potassium carbonate; zinc(II) chloride; zinc; phosphorus trichloride;
In
tetrahydrofuran; acetonitrile;
2.1: |McMurry Reaction;
DOI:10.1039/c4cc03105a
