methyl 2-methoxy-3-(2-methoxy-3-(2-methoxy-3-(2-methoxy-3-nitrobenzamido)benzamido)benzamido)benzoate

Base Information

• Chemical Name: methyl 2-methoxy-3-(2-methoxy-3-(2-methoxy-3-(2-methoxy-3-nitrobenzamido)benzamido)benzamido)benzoate
• CAS No.: 1068432-32-5
• Molecular Formula: C₃₃H₃₀N₄O₁₁
• Molecular Weight: 658.621
• Mol file: 1068432-32-5.mol

Synonyms:methyl 2-methoxy-3-(2-methoxy-3-(2-methoxy-3-(2-methoxy-3-nitrobenzamido)benzamido)benzamido)benzoate

Chemical Property of methyl 2-methoxy-3-(2-methoxy-3-(2-methoxy-3-(2-methoxy-3-nitrobenzamido)benzamido)benzamido)benzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl 2-methoxy-3-(2-methoxy-3-(2-methoxy-3-(2-methoxy-3-nitrobenzamido)benzamido)benzamido)benzoate

There total 2 articles about methyl 2-methoxy-3-(2-methoxy-3-(2-methoxy-3-(2-methoxy-3-nitrobenzamido)benzamido)benzamido)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

C25H25N3O7 (1068432-31-4) + 2-methoxy-3-nitrobenzoic acid (40751-88-0) → methyl 2-methoxy-3-(2-methoxy-3-(2-methoxy-3-(2-methoxy-3-nitrobenzamido)benzamido)benzamido)benzoate (1068432-32-5)

Guidance literature:

2-methoxy-3-nitrobenzoic acid; With oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide; for 2h; Inert atmosphere;

C₂₅H₂₅N₃O₇; With triethylamine; In dichloromethane; at 40 ℃; for 2h;

DOI:10.1021/ol801980h

Reference yield:

C25H25N3O7 (1068432-31-4) + 2-methoxy-3-nitro-benzoyl chloride (2554-86-1) → methyl 2-methoxy-3-(2-methoxy-3-(2-methoxy-3-(2-methoxy-3-nitrobenzamido)benzamido)benzamido)benzoate (1068432-32-5)

Guidance literature:

With triethylamine; In dichloromethane; at 50 ℃; for 2h; Inert atmosphere;

DOI:10.1021/ja100579z

Reference yield: 100.0%

methyl 2-methoxy-3-(2-methoxy-3-(2-methoxy-3-(2-methoxy-3-nitrobenzamido)benzamido)benzamido)benzoate (1068432-32-5) → C33H32N4O9 (1068432-33-6)

Guidance literature:

With palladium on carbon; hydrogen; In tetrahydrofuran; at 40 ℃; for 3h;

DOI:10.1021/ol801980h

upstream raw materials:

C₂₅H₂₅N₃O₇

2-methoxy-3-nitrobenzoic acid

2-methoxy-3-nitro-benzoyl chloride

Downstream raw materials:

C₃₃H₃₂N₄O₉