(2-acetyloxybenzoyl)oxymethyl 3-(3-aminopropanoyl)oxy-4-(3-nitrooxypropoxy)benzoate hydrochloride

Base Information

Chemical Name:(2-acetyloxybenzoyl)oxymethyl 3-(3-aminopropanoyl)oxy-4-(3-nitrooxypropoxy)benzoate hydrochloride
CAS No.:1248570-49-1
Molecular Formula:C₂₃H₂₄N₂O₁₂*ClH
Molecular Weight:556.911
Hs Code.:

Synonyms:(2-acetyloxybenzoyl)oxymethyl 3-(3-aminopropanoyl)oxy-4-(3-nitrooxypropoxy)benzoate hydrochloride

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Chemical Property of (2-acetyloxybenzoyl)oxymethyl 3-(3-aminopropanoyl)oxy-4-(3-nitrooxypropoxy)benzoate hydrochloride

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Technology Process of (2-acetyloxybenzoyl)oxymethyl 3-(3-aminopropanoyl)oxy-4-(3-nitrooxypropoxy)benzoate hydrochloride

There total 6 articles about (2-acetyloxybenzoyl)oxymethyl 3-(3-aminopropanoyl)oxy-4-(3-nitrooxypropoxy)benzoate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1248570-65-1
(2-acetyloxybenzoyl)oxymethyl 3-[3-(tert-butoxycarbonylamino)propanoyloxy]-4-(3-nitrooxypropoxy)benzoate

: 1248570-49-1
(2-acetyloxybenzoyl)oxymethyl 3-(3-aminopropanoyl)oxy-4-(3-nitrooxypropoxy)benzoate hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; dichloromethane; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1002/cmdc.201300105

Reference yield:

: 139-85-5
3,4-dihydroxybenzaldehyde

: 1248570-49-1
(2-acetyloxybenzoyl)oxymethyl 3-(3-aminopropanoyl)oxy-4-(3-nitrooxypropoxy)benzoate hydrochloride

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium hydrogencarbonate / acetonitrile / 4 h / 70 °C

2.1: silver nitrate / acetonitrile / 14 h / 70 °C

3.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

3.2: 3 h / 20 °C / Inert atmosphere

4.1: potassium permanganate / acetone / 1 h / 0 - 20 °C

5.1: caesium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C

6.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 3 h / 20 °C / Inert atmosphere

With hydrogenchloride; dmap; potassium permanganate; potassium hydrogencarbonate; caesium carbonate; silver nitrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1002/cmdc.201300105

Reference yield:

: 1248570-64-0
3-[3-(tert-butoxycarbonylamino)propanoyloxy]-4-(3-nitrooxypropoxy)benzoic acid

: 1248570-49-1
(2-acetyloxybenzoyl)oxymethyl 3-(3-aminopropanoyl)oxy-4-(3-nitrooxypropoxy)benzoate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C

2: hydrogenchloride / dichloromethane; 1,4-dioxane / 3 h / 20 °C / Inert atmosphere

With hydrogenchloride; caesium carbonate; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/cmdc.201300105