C₆₆H₆₄O₁₆

Base Information

• Chemical Name: C₆₆H₆₄O₁₆
• CAS No.: 353233-21-3
• Molecular Formula: C₆₆H₆₄O₁₆
• Molecular Weight: 1113.22
• Mol file: 353233-21-3.mol

Synonyms:C₆₆H₆₄O₁₆

Chemical Property of C₆₆H₆₄O₁₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₆H₆₄O₁₆

There total 3 articles about C₆₆H₆₄O₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3,4,6-tetra-O-benzoyl-α-D-galactopyranosyl trichloroacetimidate (191276-09-2) → C66H64O16 (353233-21-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 66 percent / triethylsilyl triflate / acetonitrile / -40 °C

2: 87 percent / hydrogen / PtO / methanol

3: 56 percent / bromine; tetraethylammonium bromide / dimethylformamide; CH₂Cl₂

With tetraethylammonium bromide; hydrogen; bromine; triethylsilyl trifluoromethyl sulfonate; platinum(II) oxide; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

DOI:10.1002/1521-3773(20010518)40:10<1941::AID-ANIE1941>3.0.CO;2-T

Reference yield:

D-xylal (496-62-8) → C66H64O16 (353233-21-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 66 percent / triethylsilyl triflate / acetonitrile / -40 °C

2: 87 percent / hydrogen / PtO / methanol

3: 56 percent / bromine; tetraethylammonium bromide / dimethylformamide; CH₂Cl₂

With tetraethylammonium bromide; hydrogen; bromine; triethylsilyl trifluoromethyl sulfonate; platinum(II) oxide; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

DOI:10.1002/1521-3773(20010518)40:10<1941::AID-ANIE1941>3.0.CO;2-T

Reference yield:

C39H34O12 (353233-17-7) → C66H64O16 (353233-21-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 87 percent / hydrogen / PtO / methanol

2: 56 percent / bromine; tetraethylammonium bromide / dimethylformamide; CH₂Cl₂

With tetraethylammonium bromide; hydrogen; bromine; platinum(II) oxide; In methanol; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1002/1521-3773(20010518)40:10<1941::AID-ANIE1941>3.0.CO;2-T

upstream raw materials:

2,3,4,6-tetra-O-benzoyl-α-D-galactopyranosyl trichloroacetimidate

D-xylal

C₃₉H₃₄O₁₂

Downstream raw materials:

(2R,3R,4S,5R,6R)-2-Hydroxymethyl-6-[(3R,4R)-3-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-4-yloxy]-tetrahydro-pyran-3,4,5-triol

(S)-3-Cyclohexyl-2-{(2R,3S,4S,5R,6R)-3,5-dihydroxy-2-hydroxymethyl-6-[(3R,4R)-3-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-4-yloxy]-tetrahydro-pyran-4-yloxy}-propionic acid benzyl ester