4-[(2,2-dideuterio-1-methyl)ethenyl]-1-cyclohexene-1-carboxaldehydeethylene ketal

Base Information

Chemical Name:4-[(2,2-dideuterio-1-methyl)ethenyl]-1-cyclohexene-1-carboxaldehydeethylene ketal
CAS No.:191669-67-7
Molecular Formula:C₁₂H₁₈O₂
Molecular Weight:196.258
Hs Code.:

Synonyms:4-[(2,2-dideuterio-1-methyl)ethenyl]-1-cyclohexene-1-carboxaldehydeethylene ketal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-[(2,2-dideuterio-1-methyl)ethenyl]-1-cyclohexene-1-carboxaldehydeethylene ketal

Chemical Property:

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Technology Process of 4-[(2,2-dideuterio-1-methyl)ethenyl]-1-cyclohexene-1-carboxaldehydeethylene ketal

There total 2 articles about 4-[(2,2-dideuterio-1-methyl)ethenyl]-1-cyclohexene-1-carboxaldehydeethylene ketal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18031-40-8
(S)-(-)-perillaldehyde

: 191669-67-7
4-[(2,2-dideuterio-1-methyl)ethenyl]-1-cyclohexene-1-carboxaldehydeethylene ketal

Guidance literature:: Multi-step reaction with 3 steps

1: 81.3 percent / pyridinium tosylate / benzene / 12 h / Heating

2: 1.) OsO₄, pyridine, 2.) aq. NaIO₄ / 1.) acetonitrile, 5 min, 2.) acetonitrile, 5 h

3: 1.) Ph₃P, 2.) n-BuLi

With pyridine; sodium periodate; osmium(VIII) oxide; n-butyllithium; pyridinium p-toluenesulfonate; triphenylphosphine; In benzene;
DOI:10.1002/(SICI)1099-1344(199705)39:5<369::AID-JLCR983>3.0.CO;2-F

Reference yield:

: 865-50-9
iodomethane-d3

: 191669-63-3
1-((S)-4-[1,3]Dioxolan-2-yl-cyclohex-3-enyl)-ethanone

: 191669-67-7
4-[(2,2-dideuterio-1-methyl)ethenyl]-1-cyclohexene-1-carboxaldehydeethylene ketal

Guidance literature:: With n-butyllithium; triphenylphosphine; Yield given. Multistep reaction;
DOI:10.1002/(SICI)1099-1344(199705)39:5<369::AID-JLCR983>3.0.CO;2-F